GCMS sample preparation log, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\LBA.D Vial: 24 Acq On 6 Dec 2001 10:07 pm Operator: 209 GALOS Sample 11/27 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenol, 2,2'-methylenebis[6-(1 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

32.15 0.42 ug/1 103425 Chrysene-dl2 33.01

Hit# of 5 Tentative ID MW ..-MolForm CAS# Qual

1 Phenol, 2,2‘-methylenebis[6 -(1,1-di -340 C23H3202 000119-47-1 38 2 Ethyl 4-acetylbenzoate • 192 C11H1203 038430-55-6 23 3 5-Methyl-2,4-diisopropylphenol A 192 C13H20O 000000-00-0 12 4 Phenol, 2,6-bis (1-methylpropyl) - 206 C14H220 005510-99-6 12 Abundance Scan 2953 (32.153 min): LBA.D (-) m/z 177.0,5 100.00% i 117 i 161

5000 127 340 41 57 77 91 105 — 141 , "I. 31.80 32.00 32.20 32.40 TT

—+ 4P 208 228 269 284 T TTT T m/z 161.05 70.27% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48222: Phenol, 2,2'-methylenebis[6-(1,1-dimethylethyl)-4-m 177 340

1 5000- 149 1 I 1 * 1 ' I ' ' 31.80 32.00 32.20 32.40 121 284 m/z 149.00 46.04% I • TIT 105 111 i ■ ■ • ■ i ■' ■ ■ i d r 11111111111 269• 11I •' I■ 325 i111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #20691: Ethyl 4-acetylbenzoate I 177 i TT — 1T 31.80 32.00 32.20 32.40 147 m/z 164.05 44.54% 5000 192 76 9i 121 11 1! | I I M | I i . . | I > I . | I I l t | I > I > | . I I . | 111111 ■ ■ ■ ■ i । ■ ■ ■ ■ i ■' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #20799: 5-Methyl-2,4-diisopropylphenol - • ■ i ■ ■ ■ ■ । • 1 '7 31.80 32.00 32.20 32.40 m/z 127.0,0 26.55% 5000-

192 80 107121135149 ■ ■ ।11 • • । . i > ■ ■ TIUIKguTeT 'I................ ।।।। । (. ! , • I ■ . ■ . I ■ . 1 1 1 1 1 ' I 1 1 1 'T1 m/Z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.80 32.00 32.20 32.40

LBA.D GCMS1126.M Wed Dec 12 11:39:24 2001 Page 2

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