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GCMS blank analysis for sample AE01041, Feb 2002

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GC/MS blank analysis report for sample AE01041 showing volatile organic compound results generated on February 20, 2002.

NYC-WTC_000052790–000052798

Folder label: “GCMS X 1/17/02 A 2/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1502\LBB.D Vial: 24 Acq On : 16 Feb 2002 3:42 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.43 ug/1 37187 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 36 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Silane, tetramethyl- 88 C4H12S1 000075-76-3 9 4 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 9 Abundance / Scan 345 (8.213 min): LBB.D (-) m/z 73.00 1 00.00% ( 73

5000 43 r^" 87 103 7.80 8.00 8.20 8.40 8.60 ........... l,l| ‘,lI — 1 i . ■ .55, I ' I ’ I' |' r ‘I I I | I I I I ■ | . ' ' ' i • ■ ' 1 i ‘ m/ z 42.43% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 7*3

5000 — —Ir 7.80__ 8.00 8.20 8.40 8.60 45 55 87 m/ z 45.0.5 13.80% 27 39 j ' i ■ i ' ' ' ' i ■ ' ' ' i ' । ' ' i ' ' ■ ' i ' ' ■ ■ i ' ■ ■ ■ i ■ m/Z—> _ 10 20 30 40 50 60 70 80 90 100 110 Abundance 30

7.80 8.00 8.20 8.40 8.60 5000 m/ z 41.05 11.09% )

15 41 55 70 87 m/z-> Abundance 10 20 30 40 50 60 #62932: Silane, tetramethyl- 70 73 80 90 100 110 4 7.80 8.00 ,.A ... 8.20 8.40__ 8.60 _ m/ z 39.05 8.17% 5000

45 15 | 53 59 ■ । I I > ■ | 1' >' > ■ t' । ' ' ' ' । ' 88 M m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

LBB.D GCMS0208.M Wed Feb 20 14:32:33 2002 Page 2

NYC-WTC_000052796

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NYC-WTC_000052796Source: NYC Law Department, mirrored locally

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GCMS blank analysis report, Feb 2002 · Box DEP Box 12

NYC-WTC_000005159

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

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