GCMS analysis results for sample AE03247, March 2002

NYC 9/11 Public Portal Document Llorary searcn compound xeporc

Data File : C:\MSDCHEM\1\5973N\02MAR01\03247.D Vial: 2 Acq On : 1 Mar 2002 4:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.45 ug/L 347983 Phenanthrene-dl0 22.63 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2Anthracene-D1 0 188 C14D10 000000-00-0 72, 3-F lethanol, 5-(phenylmethyl)- 188 C12H1202 000000-00-0 53 4 Cyclohexanone, phenylhydrazone $... 188 C12H16N2 000946-82-7 53 Abundance Scan 1718 (22.768 min): 03247.D (-) m/z 188.10 100.00% 188

5000 -

44 52 66 80 94 132 146 160 | 22.40 22.60 22.80 23.00

n/z-> 0- tt-| i ■ i i । I I i i । i I I i ] i i I I | i I i I | I I । । । i , i i । i rn । i i i i । I i i i । i i I i । , , If M i i । 40 50 60 70 80 I i । I Pl 90 100 110 120 130 140 150 160 170 180 190 U m/z 189.10 14.98% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 1(18

----- 5000 22.40 22.60 22.80 23.00 80 94 m/z 94.05 14.28% 66 , 158 — 0 * —Pmmmmmmmmtmp miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D10 188 - 22.40 22.60 22.80 23.00 5000 m/z 184.00 11.93% 80 94 66 160 0- ----- n miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98121:3-Furanmethanol, 5-(phenylmethyl)- 188 22.40 22.60 22.80 23.00 rn/z 80.00 10.72%

5000 141 129

mlz-> 0 ‘ I:-10‘1011101101111011110OUT“TTTUITT + II 1 1 1 i 1 " i 1 40 50 60 70 80 104

90 100 110 120 130 140 150 160 170 180 190 157 | 170 ...... - 11 22.40 22.60 22.80 23.00

)3247.D HP022102.M Mon Mar 04 12:33:22 2002 Page 14

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