GCMS analysis results for sample AE03247, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03247 conducted on March 15, 2002.

NYC-WTC_000006126–000006145

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document LlDrary bearen compound Keport

Data File : C:\MSDCHEM\1\5973N\02MAR01\03247.D Vial: 2 Acq On : 1 Mar 2002 4:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *********************************** * * * * * * ** * * * *********************** Peak Number 13 6-Methyl-7-hydroxy-8-adaman... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.06 ug/L 37316 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 6-Methyl-7-hydroxy-8-adamantylme... 332 C18H24N2O2S 000000-00-0 28 2 1,2-Benzenedicarboxylic acid, di... 330 C20H26O4 000084-61-7 9 3 1,2-Benzenedicarboxylic acid, bi... 390 C24H3804 000117-81 9 4 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26 9 Abundance Scan 2455 (31.088 min): 03247. D (-) m/z 149.00 1 00% 149

5000- 57 41 71 83 97 113 167 A. 30.80 31.00 31.20 31.40 o1 TT TT i " 1 ■ r 1111 ■1" i1"11 m/z 57.10 38.79% -n/z-> 30 40 50 60 70 80 90 100110120130 140150 160170 180 190 200 210 Abundance #282793: 6-Methyl-7-hydroxy-8-adamantylmethylthiazolo[3,2-... 83 149

93 135 5000 IT 107 30.80 31.00 31.20 31.40 67 49 m/ Z 41.10 28.21% ..... 7...... 0 TTTp-i-TTpn-rrYTTTTpn^^ . 121 11" " 1111111..... 1..... . . . H 167 " i"1 u ■ •" r H11 ■u ■ r "1 r " nz-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #281076:1,2-Benzenedicarboxylic acid, dicyclohexyl ester ... 149 ____ __ ' I ' > ' « I ' ' ' ' I ' 1 1 ' i ■ ' 30.80 31.00 31.20 31.40 5000 m/z 71.00 23.04% V 31 45 57 167 71 84 104 122 132 | | 209 0 " i" 41111111 h1 11r‘11111 ■ ■ r■" i■ I'"i ""f1" ■ i1"'r■ ‘'T" "111" I"1111 "'11 i" "'i" " lz-> 30 40 50 60 70 80 90 100110120 130 140150 160 170 180 190 200 210 Abundance #326907:1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) e... ' I ' ' - 1 I 1 1 ' 1 i ■ ■ 1 ' i ' 1 149 30.80 31.00 31.20 31.40 m/ Z 55.10 22.30%

5000 57 167 71 83 , A113

m/z-> 0 mH 42 m—mmmm I I 93 ,4 ll TOTTgn 30 40 50 60 70 80 90 100110120 130 140 150 160170 180 190 200 210 11 1 * ‘ ' 1 11 30.80 31.00 31.20 31.40 1 ■ i ■ ■

)3247.D HP022102.M Mon Mar 04 12:33:22 2002 Page 15

NYC-WTC_000006144

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