VOC analysis results, sample AE10023, April 30, 2002

NYC 9/11 Public Portal Document uiorary bearen compound Report Data File : C:\MSDCHEM\l\5973N\02APR30\10025.D Vial: 9 Acq On : 30 Apr 2002 6:40 pm Operator: Sample : nyc Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSC.P Quant Method : C:\MSDCHEM\1...\W042302.M (RTE Integrator) Title : VOC method 8260 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 1,6-Hexanediol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 33.78 0.03 ug/L 16394 1,4-Dichlorobenzene-d4 31.55 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,6-Hexanediol 118 C6H14O2 000629-11-8 38 2 7-Oxabicyclo[4.1.0]heptan-2-ol 114 C6H10O2 001192-78-5 37 3 2-Ethylhexylfumaroyl monochloride 246 C12H19C1O3 000000-00-0 37 4 2,4-Dimethyl-1-heptene 126 C9H18 019549-87-2 32 Abundance Scan 3034 (33.784 min): 10025.D (-) m/z 42795 100700% 43 7P 55

5000

135 , A Mr I Ift^A , A, 83 33 40 33.60 33.80 34.00 34.20 0 Tp-rrTp-rTTy m/z TOTOO 92.66% TiZz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210220 '\bundance #17768; 1,6-Hexanediol 1 42

5000 57 67 33 40 33.60 33.80 34.00 34.20 82 m7z 55.00 64.83% 0 I IMii TrpWprriprrTjtTnT I ' I" " I JTTTTpTTTJTTrrpTTrpTTT^ nZz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #15033: 7-Oxabicyclo[4.1.0]heptan-2-ol 5(7 7p

39 33'40' 'saeo' '33.80' '34'00' '34'20' 5000 27 m/z 56790 51.53%

.. I 0 Tp-rrvp-n-q- TTryrr? 96 ■I............. ................. I" " I" ‘' I r "' I I' I" " I T)/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210220 Abundance #180921: 2-Ethylhexylfumaroyl monochloride ,, ______ 57 33 40 33.60 33.80 34.00 34.20 70 inTz sYTTO 50.76% 5000 27

83 42 0 nn/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180190200210220 33.40 33,60 33.80 34.00 34.20

.0025.D W042302.M Wed May 01 14:36:08 2002 Page 6

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