GCMS analysis results, sample AE02785, March 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE02785 performed on 3/11/2002, detecting 2,4-DDD and other unknown compounds.

NYC-WTC_000005545–000005563

Folder label: “GCMS X 2/6/02 A 3/1/02”

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NYC 9/11 Public Portal Document ulpraIY bearcIl compourd KepOL

Data File C:\HPCHEM\l\DATA\MAR0102\2785.D Vial: 19 Acq On 2 Mar 2002 2:03 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Naphthalene, 1,7-dimethoxy- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.22 ug/1 30145 Phenanthrene -dl0 25.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 59 2 4-Methyl-2-(4-flyorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 53 3 4-Methyl-2-(3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 53 4 Anthracene-d10- 7 188 C14D10 m/z 18 8.10 _ 100.00% 50 001719-06-8 Abundance ' .. ”..................Scan 2266 (25.847 min): 2785.D (-)..................................... ......... 1$8

5000 - — 80 94 158 . 25.60 25.80 26.00 26.20 ......... 611 1111 ■1111" ।'11111 ■'11" " ।11" ।111 h1111111" i11,’ I r TTT m/z 184.10 14.93% m/Z-> 40 Abundance 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #19913: Naphthalene, 1,7-dimethoxy- 173 188 ;. 1 5000 -----PPPP 115 25.60 25.80 26.00 26.20 102 145 m/ z 94.00 12.40% 51 63 75 94 ; 130 158 l.. ... ' ■ I ' ' ' ' i 1 1 I 1 ' 1 1 1 1 1 1 1 1 ■ ' 1 ■ ■ ■ ■ 1 1 1 1 1 ! ' 111 11 ' I ' 1 i' ■'' i' m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance . . , 188 ................ .......................... 121 25.60 25.80 26.00 26.20 5000 m/ z 18 .10 11.08% 173 67 94 57 75 102 146 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19859: 4-Methyl-2-(3-fluorophenyi)pyrimidine 188 25.60 25.80 26.00 26.20 m/z 79.95 10.61% 5000- 121

67 94 173 ......... 175..... 91....... I 1'!' ' 1' I ' '1111 1 1' 111'' I ‘ 1'11 *1 ‘11' ■1 ■ i1 ■' ■ i11111111111T1 111 ■ 11 >'i 11111 146 161 I I T’T nvz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2785.D GCMS0208.M Tue Mar 05 10:50:28 2002 Page 1

NYC-WTC_000005552

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