GCMS analysis results, sample AE02785, March 2002

NYC 9/11 Public Portal Document Llbrary Searcn compound Keport

Data File C:\HPCHEM\1\DATA\MAR0102\2785.D Vial: 19 Acq On 2 Mar 2002 2:03 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 1,2-Benzenedicarboxylic acid, Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

27.68 0.22 ug/1 29104 Phenanthrene-dl0 25.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, butyl 304 C18H24O4 000084-64-0 83 2 1,2-Benzenedicarboxylic acid, butyl 278 C16H2204 017851-53-5 83 3 Bis(2-methoxyethyl) phthalate 282 C14H1806 000117-82-8 83 4 Dibutyl phthalate 278 C16H2204 000084-74-2 (83 Abundance Scan 2466 (27.683 min): 2785.D (-) m/z.149.00.100.00% 149

5000

1 ‘ I 1 ' ‘ I ' 1 41 57 76 104 । 205 223 27.40 27.60 27.80 28.00 -----HP ' i ■ ■ ' ' i ' ' ' ' i ■ ■ ' ' i ' 1 ‘ ' i ' i■ i ■ ■ ■ ■ i ■ ■ ' ■ i 1 m/z 149.90 9.00% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #43452: 1.2-Benzenedicarboxylic acid, butyl cyclohexyl ester 149

5000 27.40 27.60 27.80 28.00 m/z 41.05 7.46% 55 67 83 104 121 167 205 223 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 149

27.40 27.60 27.80 28.00 5000 m/ z 57.0,0 4.87%

27 41 57 76 104 121 205 223 278 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39720: Bis(2-methoxyethyl) phthalate 149 27.40 27.60 27.80 28.00 m/z 56.0.0 4.44% 5000

41 57 76 104 121 205 223 .................... .. r1 1 1 1 1 1 ’ ' • | ■ 1 | | > . . . | . ■ > . | . . . . | . ■ , ■ | | | l | >' | I I J | J , ' , ' | | | | I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 27.40 27.60 27.80 28.00

2785.D GCMS0208.M Tue Mar 05 10:50:33 2002 Page 2

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