GCMS analysis results for sample AE02786, March 11, 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02786 showing unknown compounds and surrogate recovery data from March 11, 2002.

NYC-WTC_000005564–000005573

Folder label: “GCMS X 2/6/02 A 3/1/02”

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NYC 9/11 Public Portal Document ULJLaLY OCa-Uii totupOult RCPOL L

Data File C:\HPCHEM\1\DATA\MAR0102\2786.D Vial: 20 Acq On 2 Mar 2002 3:02 am Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Naphthalene, 1,7-dimethoxy- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

25.86 0.25 ug/1 30848 Phenanthrene-dl0 25.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Naphthalene, 1, 7-dimethoxy- 188 C12H1202 005309-18-2 45 2 4 - Fluoro- 6 -methyl - 2 -phenylpyrimidin 188 C11H9FN2 000000-00-0 42 3 Phenant hrene-d10 X WD 188 C14D10 001517-22-2 40 4 Anthracene -10- 7 9 188 C14D10 001719-06-8 39 Abundance......... 7..... Scan 2267 (25.856 min): 2786.D (-).. m/z 188.10 100.00% 188

5000- /.......... 1 1 i ■' ■ ■ 1 1 ■ ■ ■ i 1'1 1 1 1 1 1 80 94 I _ 25.60 25.80 26.00 26.20 44..........66 m***mmmmmmm TIP .................................................................................... m/z 189.05 17.76% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ] Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188 ........................... ................... 5000 115 25.60 25.80 26.00 26.20 102 145 m/z 156.05 13.05% 51 63 75 94 130 158 '' i ■ ■'' i'''' i■11'' ■ ‘ i'' ■ ■ i ■ । ■ ' ■ i'1 “ i'" ■ i ■1 " i11111111' 1111111' " I " 1 '111 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188

25.60 25.80 26.00 26.20 5000- m/z 80.05 11.24% 85 103 51 77 173 94 114 m/z-> ............................................... 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-di 0 188 25.60 25.80 26.00 26.20 m/ z 94.00 9.60% 5000

80 94 160 ............................................... 66 ■ ■ i11 ■' । “111111111" 'I‘ ‘i ' i " ' ■ i'1 " I' " 1111 " I " 1111' 111 " 11111111 l It" m/z-> 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2786.D GCMS0208.M Tue Mar 05 10:51:58 2002 Page 1

NYC-WTC_000005571

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NYC-WTC_000006328

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