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GCMS analysis results for sample AE02600, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02600 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005312–000005321

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005320
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NYC 9/11 Public Portal Document j_ij.jui.cixy DEdLti LotLpOuLU RCDOL L

Data File C:\HPCHEM\l\DATA\MAR0102\2600.D Vial: 10 Acq On 1 Mar 2002 5:13 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.86 0.28 ug/1 31861 Phenanthrene-dl0 25.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-diO /7 188 C14D10 001517-22-2 72 2 3-Quinolinecarbo le, 1,2,3,4-te 188 C10H8N2O2 022384-05-0 59 3 Naphthalene, 17-dimethoxy- 188 C12H1202 005309-18-2 45 4 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 40 Abundance / Scan 2267 (25.858 min): 2600.D (-) i m/z 188.10 100.00% i $8

5000 ............................. ................. 56 78 94 158 25.60 25.80 26.00 26.20 mHPP — m/z 65.95 19.02% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-dlO 188

................................ 5000 25.60 25.80 26.00 26.20 : m/ z 78.15 15.92% ■ ■ ■ ' J ' ■ ■ ■ | 66 । T | ' ■ ■ ' ................ 94 | | | | | J60 | I ■ I 1 | I I I I | I I ! ! TMH I I m/z-> 40 50 60 70 80 90 100 110 120 130 140150 160 170 180 190 Abundance 188

128 172 25.60 25.80 26.00 26.20 93 m/ z 80.05 12.42% 5000- 117 142 66

m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188 25.60 25.80 26.00 26.20 m/z 94.00 12.27% 5000 115 145 102 51 63 75 94 130 ' 1 i ' r' ' i ,f| 1 ' I 1 '''111 11 11 111' I >< । । । ■ PP ... ..... 158...... 1..... 1 1 11 111 11 ' 1 1 1 1 1 1 11 1 1 1 1 11 -p-T 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2600.D GCMS0208.M Mon Mar 04 11:44:27 2002 Page 2

NYC-WTC_000005320

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NYC-WTC_000005320Source: NYC Law Department, mirrored locally

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