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GCMS analysis results for sample AE02600, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02600 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005312–000005321

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005319
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document ILJL CL Y wuptiit ISPJ

Data File C:\HPCHEM\1\DATA\MAR0102\2600.D Vial: 10 Acq On 1 Mar 2002 5:13 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.35 ug/1 28318 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 9 3 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 9 4 Formamide/ N,N-dimethyl - 73 C3H7NO 000068-12-2 100.00% 5 Abundance / Scan 343 (8.195 min): 2600.D (-) ' m/ z 73.00 3

5000 43 II* '^1 11 39 57 09 7.80 8.00 8.20 8.40__ 8.60 TTTTTTTTTTTTTTTTTTTTTTTTTTTTTT 49 TI0- " 'I'1'11" " i' -HH 11PP] 84 87 ' " I'1" I' ‘‘ I' m/z 43.05 27741% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #292: N-Ethylformamide 30

5000 73

■ i ■ ■ • ■ i ■ ■ ■ > । 7.80_ 8.00 8.20 A ■ 8.40 8.60 44 58 27 ! m/z 41.05 11.64%

m/z-> 5 .... 15...... inj .. A1l 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ' i " 1 ■ r ■ 1 r ''11 " " r '11 r ■1 ■ i ■ ‘ " i " 1 ■ r ■ ■111

Abundance 73

55 7.80 8.00 8.20 8.40 8.60 43 5000 m/z 44.95 11.59% 27 31 70 81 '' I' " ' I " '' I'' " I'11' I' ■ i ■ ■ ■ ■ । > i1 ■ ‘11 ■ • ■1 >b ‘" i ■ ■ ■ ■ i ■1 ■ ■ i ■1 ■ ■ i • ■ ■ ■ i • ■ • ■ i > ■ ■ ■ i ■ ■ ■ ■ i ■ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63573: 3-Pentanol, 3-methyl- 73 7.80 8.00 8.20 8.40 8.60 m/z 71.0.0 7.46% 5000 55 __________ 27- 31 ,41, 45 69 87

m/z-> mWPTPTTTTT 5 10 15 20 25 30 35 40 " i" 45 50 55 . . 84.1. ■ t ■ ■ ■ 11 ■ ■ ■11 ■ ■ 60 65 70 75 80 85 90 95 i-rp- 7.80 8.00 8.20 8.40 8.60

2600.D GCMS0208.M Mon Mar 04 11:44:23 2002 Page 1

NYC-WTC_000005319

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NYC-WTC_000005319Source: NYC Law Department, mirrored locally

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