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GCMS analysis results for sample AE00845, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE00845 conducted on February 11, 2002, including surrogate recovery data.

NYC-WTC_000005202–000005209

Folder label: “GCMS X 2/4/02 A 2/8/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\00845.D Vial: 11 Acq On 8 Feb 2002 7:04 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.350 790 796 807 rVB 765669 1887888 76.76% 15.374% 2 15.995 1186 1193 1210 rBV 1118158 2326590 94.60% 18.946% 3 21.310 1765 1772 1783 rBV 1202777 2459480 100.00% 20.029% 4 25.754 2250 2256 2267 rBV2 1118993 2367335 96.25% 19.278% 5 30.830 2805 2809 2816 rBV 141003 268786 10.93% 2.189%

6 33.823 3129 3135 3150 rBV2 774652 1706492 69.38% 13.897% 7 38.110 3594 3602 3617 rBV2 425163 1263240 51.36% 10.287%

Sum of corrected areas: 12279811

00845.D GCMS0208.M Mon Feb 11 12:29:09 2002

NYC-WTC_000005207

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NYC-WTC_000005207Source: NYC Law Department, mirrored locally

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