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GCMS analysis results for sample AE02967, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02967 showing unknown compounds and surrogate recovery data from February 15, 2002.

NYC-WTC_000005642–000005650

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\2967.D Vial: 31 Acq On 9 Feb 2002 2:28 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.213 341 345 359 rBV 119167 284090 9.19% 1.874% 2 12.344 789 795 806 rBV 1041268 2301600 74.45% 15.185% 3 15.989 1186 1192 1208 rBV 1472222 2877680 93.08% 18.986% 4 21.304 1764 1771 1783 rBV 1572326 3091636 100.00% 20.397% 5 25.757 2249 2256 2267 rBV 1410867 2955596 95.60% 19.500%

6 30.824 2803 2808 2814 rBV 160315 322076 10.42% 2.125% 7 33.817 3128 3134 3151 rBV2 851993 1967346 63.63% 12.980% 8 38.104 3593 3601 3618 rBV2 449752 1357145 43.90% 8.954%

Sum of corrected areas: 15157169 2967.D GCMS0208.M Wed Feb 13 11:08:21 2002

NYC-WTC_000005647

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NYC-WTC_000005647Source: NYC Law Department, mirrored locally

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