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GCMS analysis results for sample AE02970, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02970 showing unknown compounds and surrogate recovery data from February 15, 2002.

NYC-WTC_000005669–000005678

Folder label: “GCMS X 2/7/02 A 2/9/02

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Scanned page image, NYC-WTC_000005674
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\2970.D Vial: 34 Acq On 9 Feb 2002 5:23 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.214 341 345 359 rBV 84510 258270 8.35% 1.654% 2 8.370 359 362 373 rVB 15748 43561 1.41% 0.279% 3 12.345 790 795 807 rVB 930617 2272175 73.47% 14.549% 4 15.989 1186 1192 1208 rBV 1428640 2819140 91.15% 18.051% 5 21.305 1764 1771 1782 rBV 1545512 3092768 100.00% 19.803%

6 25.757 2249 2256 2267 rBV 1422197 2961156 95.74% 18.960% 7 30.825 2803 2808 2814 rBV 171859 338270 10.94% 2.166% 8 33.827 3126 3135 3152 rBV 964656 2209026 71.43% 14.144% 9 38.114 3593 3602 3619 rBV2 534336 1623204 52.48% 10.393%

Sum of corrected areas: 15617570

2970.D GCMS0208.M Wed Feb 13 11:10:26 2002

NYC-WTC_000005674

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NYC-WTC_000005674Source: NYC Law Department, mirrored locally

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