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GCMS analysis results for sample AD31132, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31132 conducted on February 11, 2002, including surrogate recovery data.

NYC-WTC_000005229–000005238

Folder label: “GCMS X 2/4/02 A 2/8/02

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Scanned page image, NYC-WTC_000005234
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C: \HPCHEM\ 1 \DATA\ FEB0802\31132.D Vial: 14 "Acq On 8 Feb 2002 9:59 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.261 130 133 138 rBV 12679 24393 1.04% 0.208% 2 12.348 790 796 808 rVB 705222 1756942 74.78% 15.003% 3 15.993 1187 1193 1203 rBV 1067636 2171448 92.43% 18.543% 4 21.308 1765 1772 1786 rBV 1144960 2349369 100.00% 20.062% 5 25.237 2198 2200 2202 rBV 43816 24573 1.05% 0.210%

6 25.751 2250 2256 2268 rBV2 1040152 2276320 96.89% 19.438% 7 30.828 2805 2809 2815 rVB 125204 241626 10.28% 2.063% 8 33.821 3129 3135 3155 rBV2 742918 1665794 70.90% 14.225% 9 38.108 3595 3602 3622 rBV2 405176 1200117 51.08% 10.248%

Sum of corrected areas: 11710582

31132.D GCMS0208.M Mon Feb 11 12:31:33 2002

NYC-WTC_000005234

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NYC-WTC_000005234Source: NYC Law Department, mirrored locally

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