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GCMS analysis results, sample AE03015, February 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE03015 conducted on 2/15/2002, detecting 2,4-DDD and other unknown compounds with specified detection limits.

NYC-WTC_000005716–000005724

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\3015.D Vial: 39 Acq On 9 Feb 2002 10:13 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.218 342 346 373 rVB 111257 321463 9.35% 1.832% 2 12.349 790 796 809 rVB 1077509 2534750 73.76% 14.441% 3 15.994 1186 1193 1209 rBV 1545933 3182156 92.60% 18.130% 4 21.309 1765 1772 1788 rBV 1687139 3436573 100.00% 19.580% 5 25.752 2249 2256 2267 rBV2 1566290 3331446 96.94% 18.981%

6 30.829 2804 2809 2815 rVB 193733 370058 10.77% 2.108% 7 33.822 3127 3135 3153 rBV2 1125257 2509043 73.01% 14.295% 8 38.109 3593 3602 3618 rBV2 620019 1866373 54.31% 10.633%

Sum of corrected areas: 17551862

3015.D GCMS0208.M Wed Feb 13 11:13:56 2002

NYC-WTC_000005721

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NYC-WTC_000005721Source: NYC Law Department, mirrored locally

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