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GCMS analysis results, Feb 2002

Machine-extracted title · confidence 95%

Laboratory report showing GCMS detection of unknown compounds and surrogate recovery for sample AD31586 on February 11, 2002.

NYC-WTC_000005167–000005175

Folder label: “GCMS X 2/4/02 A 2/8/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

’ Data File C:\HPCHEM\l\DATA\FEB0802\31586.D Vial: 7 Acq On 8 Feb 2002 3:09 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.276 130 134 141 rBV 18462 36411 1.31% 0.271% 2 12.353 790 796 808 rVB 868579 2055428 73.90% 15.291% 3 15.988 1186 1192 1203 rBV 1219380 2506933 90.13% 18.650% 4 21.313 1765 1772 1786 rBV 1333616 2781381 100.00% 20.692% 5 25.756 2249 2256 2267 rBV2 1248369 2589997 93.12% 19.268%

6 30.833 2805 2809 2816 rVB 171651 322328 11.59% 2.398% 7 33.826 3129 3135 3149 rBV2 833391 1820364 65.45% 13.542% 8 38.113 3595 3602 3617 rBV2 445451 1329057 47.78% 9.887%

Sum of corrected areas: 13441899

31586.D GCMS0208.M Mon Feb 11 12:32:53 2002

NYC-WTC_000005172

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NYC-WTC_000005172Source: NYC Law Department, mirrored locally

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