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Document / 9 pages

GCMS analysis results for sample AD31252, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD31252 conducted on February 11, 2002, including surrogate recovery data.

NYC-WTC_000005210–000005218

Folder label: “GCMS X 2/4/02 A 2/8/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File C:\HPCHEM\l\DATA\FEB0802\31252.D Vial: 12 Acq On 8 Feb 2002 8:02 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.268 129 133 137 rBV 16796 32084 1.30% 0.267% 2 12.345 790 795 806 rVB 796199 1906804 77.01% 15.881% 3 15.990 1186 1192 1209 rBV 1187765 2348950 94.87% 19.563% 4 21.305 1765 1771 1781 rBV 1240344 2476039 100.00% 20.622% 5 25.757 2249 2256 2267 rBV2 1142373 2362391 95.41% 19.675%

6 30.834 2804 2809 2816 rVB 147582 271691 10.97% 2.263% 7 33.827 3128 3135 3146 rBV 717357 1561571 63.07% 13.006% 8 38.114 3593 3602 3619 rBV2 360218 1047302 42.30% 8.723%

Sum of corrected areas: 12006832

31252.D GCMS0208.M Mon Feb 11 12:32:15 2002

NYC-WTC_000005215

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NYC-WTC_000005215Source: NYC Law Department, mirrored locally

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