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GCMS analysis results for sample AE02968, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02968 showing unknown compounds and surrogate recovery data from February 15, 2002.

NYC-WTC_000005651–000005659

Folder label: “GCMS X 2/7/02 A 2/9/02

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Scanned page image, NYC-WTC_000005656
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\2968.D Vial: 32 Acq On 9 Feb 2002 3:27 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.214 341 345 359 rBV 110381 277191 8.76% 1.720% 2 12.345 790 795 810 rVB 1042678 2315987 73.16% 14.369% 3 15.989 1186 1192 1209 rBV 1481387 2888349 91.24% 17.921% 4 21.305 1765 1771 1784 rBV 1571762 3165665 100.00% 19.641% 5 25.757 2249 2256 2268 rBV 1482710 3058447 96.61% 18.976%

6 30.834 2804 2809 2814 rVB 163240 321827 10.17% 1.997% 7 33.827 3128 3135 3152 rBV 1055911 2312848 73.06% 14.350% 8 38.114 3593 3602 3618 rBV2 586815 1777181 56.14% 11.026%

Sum of corrected areas: 16117495

2968.D GCMS0208.M Wed Feb 13 11:09:00 2002

NYC-WTC_000005656

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NYC-WTC_000005656Source: NYC Law Department, mirrored locally

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