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← Document results/DEP Box 12/GCMS X 2/7/02 A 2/9/02
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GCMS analysis results for sample AE02973, February 2002

Machine-extracted title · confidence 100%

Laboratory report for DEP sample AE02973 showing unknown compounds and surrogate recovery data from February 15, 2002.

NYC-WTC_000005689–000005697

Folder label: “GCMS X 2/7/02 A 2/9/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\FEB0802\2973.D Vial: 37 Acq On 9 Feb 2002 8:17 pm Operator: 209 GALOS Sample GC/MS SCAN 2/7FB Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.222 341 346 361 rBV 127057 351946 9.62% 1.926% 2 12.344 789 795 810 rBV 1113332 2649879 72.46% 14.503% 3 15.988 1186 1192 1208 rBV 1713730 3328642 91.02% 18.218% 4 21.304 1764 1771 1791 rBV 1792689 3656923 100.00% 20.014% 5 25.756 2249 2256 2266 rBV 1701734 3458310 94.57% 18.927%

6 30.833 2804 2809 2815 rVB 193428 383938 10.50% 2.101% 7 33.826 3128 3135 3153 rBV 1157976 2549303 69.71% 13.952% 8 38.113 3593 3602 3622 rBV 627858 1892500 51.75% 10.358%

Sum of corrected areas: 18271441

2973.D GCMS0208.M Wed Feb 13 11:12:40 2002

NYC-WTC_000005694

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NYC-WTC_000005694Source: NYC Law Department, mirrored locally

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