GCMS unknown compounds report, Feb 25, 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\FEB1102\892.D Vial: 37 Acq On : 12 Feb 2002 11:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 8.222 342 346 351 rBV 11835 26637 1.33% 0.263% 2 12.344 790 795 810 rVB 601478 1532818 76.44% 15.143% 3 15.989 1186 1192 1210 rBV 931103 1867300 93.12% 18.447% 4 21.304 1765 1771 1786 rBV 1021410 2005328 100.00% 19.810% 5 25.757 2249 2256 2267 rBV2 916714 1943808 96.93% 19.203%

6 30.833 2804 2809 2814 rVB 157281 290923 14.51% 2.874% 7 33.826 3128 3135 3147 rBV 659290 1454379 72.53% 14.368% 8 38.113 3594 3602 3618 rBV 330232 1001365 49.94% 9.892%

Sum of corrected areas: 10122558

892.D GCMS0208.M Wed Feb 20 09:48:15 2002

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