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GCMS analysis results, Feb 2002

Machine-extracted title · confidence 95%

Laboratory report showing GCMS detection of unknown compounds and surrogate recovery for sample AD31640 on February 11, 2002.

NYC-WTC_000005176–000005183

Folder label: “GCMS X 2/4/02 A 2/8/02

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OCR text

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NYC 9/11 Public Portal Document

LSC Area Percent Report

■ Data File C:\HPCHEM\1\DATA\FEB 0802\31640.D Vial: 8 Acq On 8 Feb 2002 4:07 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.351 790 796 809 rVB 726617 1729002 75.52% 15.818% 2 15.996 1186 1193 1210 rBV 1018448 2120334 92.62% 19.398% 3 21.311 1765 1772 1784 rBV 1142374 2289364 100.00% 20.944% 4 25.754 2250 2256 2267 rBV2 1003429 2121446 92.67% 19.408% 5 30.831 2805 2809 2815 rBV 124936 240427 10.50% 2.200%

6 33.824 3129 3135 3147 rBV2 659603 1416376 61.87% 12.958% 7 38.111 3594 3602 3617 rBV2 344365' 1013885 44.29% 9.275%

Sum of corrected areas: 10930834

31640.D GCMS0208.M Mon Feb 11 12:33:23 2002

NYC-WTC_000005181

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NYC-WTC_000005181Source: NYC Law Department, mirrored locally

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