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GCMS analysis results, sample AE00831, February 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE00831 performed on 2/11/02, detecting unknown compounds and 2,4-DDD surrogate at 81 ug.

NYC-WTC_000005194–000005201

Folder label: “GCMS X 2/4/02 A 2/8/02”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\FEB0802\00831.D Vial: 10 Acq On 8 Feb 2002 6:05 pm Operator-: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.351 790 796 808 rVB 713027 1793157 75.41% 15.404% 2 15.987 1186 1192 1206 rBV 1054959 2204912 92.72% 18.941% 3 21.311 1765 1772 1788 rBV 1171627 2378009 100.00% 20.428% 4 25.755 2250 2256 2267 rBV2 1073395 2265223 95.26% 19.460% 5 30.831 2805 2809 2815 rVB 129324 248494 10.45% 2.135%

6 33.824 3128 3135 3148 rBV2 728198 1620159 68.13% 13.918% 7 38.111 3594 3602 3620 rBV2 379761 1130706 47.55% 9.713%

Sum of corrected areas: 11640660

00831.D GCMS0208.M Mon Feb 11 12:28:43 2002

NYC-WTC_000005199

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NYC-WTC_000005199Source: NYC Law Department, mirrored locally

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