DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB01\0129B.D Vial: 1 Acq On : 1 Feb 2002 10:35 am Operator: Sample : lab blank 1/29 Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ******************** * *** * * * ****************************************** Peak Number 3 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.92 0.41 ug/L 160678 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -(CYCLOHEX-3'-EN-YL)PROPANOL $$ . . . 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 28 4 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 28 Abundance Scan 223 (5.920 min): 0129B.D (-) m/z 73.10 100.00% 73

5000 43 ' ' ' i ' ' ' ' i ' ' ' ‘ i ' ' ' ■ i ' ■ ■ • i 5.60 5.80 6.00 6.20 . .. I,1 , 59 , 11 0- 1 I' 1 11 I'1'' I 11''111 11 I 11 1 'T1 ! 87 103 1IIIP9mmmm]mmmmmT] m/z 43.10 25.30% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 1 1 n 111 i1 1 ' 1 i 1 ■' ' i 5.60 5.80 6.00 6.20 43 m/ z 41.10 8.73% 27 55 , 87 113 174 0--- 11 " ■ ■ i ■11 ’I’ 1 ....... . I ' ' ' ....... | I‘I I I | I >! I | I I I I | I I I I | I I I I | I I I I | I I J I | ' n/z- > 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 ' ' ' I........1 ' I ' ' I ' I 1 1 I I 5.60 5.80 6.00 6.20 5000 m/ z 45.10 8.73% 43 27 55 87 113 174 0- ' I 1 1 ''' I 1 1 1 ' l'1 1 1 111111111 1 'T' TT1‘"‘‘1‘111111110UETTTTTmTTEIETITT‘""31"1S11" m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #9702: Butahe, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 1 ' ■ i ■ ■ ■ r i ■ ■ ■' ■ i 1 1 1 1 i 1 1-1 ' i 73 5.60 5.80 6.00 6.20 m/z 71.10 6.07% / 5000

55 87

n/z-> 27 45 I 0 ' i''' ‘ i ■ “ ' i ■ " 11 " 20 30 40 50 + —mTTTIPTTTTTT 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20 1II

0129B.D SCAN508.M Mon Feb 04 08:40:58 2002 Page 5

NYC-WTC_000003999

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NYC-WTC_000003999Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999