GCMS analysis results, Feb 27 2002

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Laboratory report showing GC/MS analysis results for sample AE01136 testing unknown compounds and specific analytes on February 27, 2002.

NYC-WTC_000003444–000003462

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02FEB25\01136.D Vial: 3 Acq On : 25 Feb 2002 12:53 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 6 1-Propene-1-thiol Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.95 0.50 ug/L 206580 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propene-l-thiol 74 C3H6S 000925-89-3 23 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 17 3 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 17 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 228 (5.948 min): 01136. D (-) m/ z 73.10 100.00% 70

5000 43 -

5.60 5.80 6.00 6.20 55 11 1.. ......... .. . 0 ............ nW ' ‘ I ' ' ' 1 I ' ‘ ' 1 1 TT T1" m/z 43.10 27.30% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #2002:1 -Propene-1 -thiol 70

5000 111111 1f 5.60 5.80 6.00 6.20 43 m/z 41.10 9.20% — O-TTTT 11' • * 11 < ’ I s‘ ‘‘I‘‘‘T4 T’ mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 341,3]dioxolan-2-ylpropyl ester 70 ........... HI}............ 5.60 5.80 6.00 6.20 5000 m/z 45.10 8.20% 43 27 55 87 113 174 0 -Tt < । > • ■ ■ । << > । > Ij • 11 —hmP— T—n1I—m00mm00‘T i ■ ■' ■ i ■ m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... ■ ' i ■ ' ■ ■ i 1 ' ' 1 i ‘ • i ' 1 ■ ' i ' 70 5.60 5.80 6.00 6.20 m/z 71.00 7.90% 5000 43 27 55 87 113 174 0 —P 1 r ■111 ■11 ■ r l ■ ■ । ■ PuUTmT I''' 'I 111 "TI r 1" i ■ T’ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

01136.D HP022102.M Tue Feb 26 08:29:56 2002 Page 8 NYC-WTC_000003455

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NYC-WTC_000003455Source: NYC Law Department, mirrored locally

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