DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02015.D Vial: 3 Acq On : 26 Feb 2002 11:57 am Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.95 0.22 ug/L 105393 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 1-Propene-1-thiol 74 C3H6S 000925-89-3 5 Abundance Scan 228 (5.948 min): 02015.D (-) m/ z 73.10 100.00% 73

5000 43 ....... I ...... ......... 5.60' 1 5.80 ' i 1 ' ■ 1 i 1 1 1 n ' 1 1 1 i 1 6.00 6.20 87 103 O-T ..... . ...... . ................ .. —— DamuuuOTmTPPPTPTT) 1 ‘ " 1 I'1 " I 111' I ' ‘ " I 1' 1 'T' m/ z 43.10 22.50% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 A Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 ------------------------ 5,60 5.80 6.00 6.20 43 m/z 45.10 8.96% 27 55 ,i , 87 113 174 01111 ■1 " i1 " ' i1 1 1 1 i'1 1 ■ ■ । । i'i । । । > 1 i'i । 2‘0100011191101000200010m0Tpap miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 1 1 i ■ ■ 1 1 1 1 1 ' 1 I1 1 1 1 I 1 1 1 1 1 1 5.60 5.80 6.00 6.20 5000 m/ z 41.10 8.34%

43 27 55 , 87 113 174 0 TTr ‘1’41’1’11 'T1 T‘—E—0-—10T0ET0uumug , I

mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... —' ' i ■ ■ 1 ■ i ■ ' ' 1 । ' fi >-| । । । । । । 30 5.60 5.80 6.00 6.20 73 m/z 71.00 6.09% 5000 44 58

15 0 " I' 1 r ’1 'i ■ " 11'11 ■ ■ । ■1411 ■■ ■ ■ i " " i "1' i " ‘1111 •111111111" I ■ ‘ " 11ITITT ‘ ■ i ' ' ' ' i ' ' ' ' i ' ‘ ' i ■ ' ' ‘ i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

02015.D HP022102.M Wed Feb 27 08:34:25 2002 Page 8

NYC-WTC_000004556