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GC/MS analysis results for sample AD23834, Nov 1 2001

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Laboratory report documenting GC/MS analysis of sample AD23834 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089476–000089500

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089485
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NYC 9/11 Public Portal Document

Library Search Compound Report Lata File : C;\HPCHEM\1\DATA\OCT3001\23834.D Vial: 19 Acq On : 31 Oct 2001 8:04 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00. MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L * * * ****************************************************************** Peak Number 3 3-Hexanol Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 6.57 0.49 ug/1 73009 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol/ 102 C6H14O 000623-37-0 74 2 Amylene yHydrate 88 C5H12O 000075-85-4 ,38 3 2-Prop^ol, 2-methyl- 74 C4H10O 000075-65-0 36 4 l-Hept;4n-4-ol 114 C7H14O 003521-91-3 -10 Abundance 7 Scan 166 (6.565 min): 23834.D (-) 5b m/z 59705 100.00%

5000- 73 43 620 6.40 6.60 6.80 7.00 I'l I ' ' ' ■ I I ; ■ ■ I I 85 m/z 55.00 87.00% ■nZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63529:3-Hexanol 5)9

31 5000 73 6.20 6.40 6.60 6.80 7.00 m/z 73.00 46703% 44 ■ ........................................ l‘ .. 102 --t+ ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62940: Amylene Hydrate

6.20 6.40 77'./-;; 6.60 6.80 7.00 73 5000 45 m/z 43.00 24.86% 31 ------------ -------------- -|- n-r+ ' I ' ''''''I 70 ' 80' ' ' '90' ' ' 100 ' ' 110 Ti/z-> 10 20 30 40 50 60 Abundance #62575:2-Propanol, 2-methyl- - 6.20 ~6.4OJi6'.6O - eso 17.00 "mTz 41.05 23.40%

5000- 31 41 15 I —I—r-n—]—r-r-ri—p 1 Tl/i-> 10 20 30 40 50 60 70 80 90 10b 110 6.20 6.40 6.60 6.80 7.00

I

23834.D NP103001.M Thu Nov 01 13:21:30 2001 Page 3

NYC-WTC_OO6O89485

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NYC-WTC_000089485Source: NYC Law Department, mirrored locally

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