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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089316
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C;\HPCHEM\1\DATA\OCT3001\23799.D Vial: 10 Acq On ; 30 Oct 2001 11:19 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params; LSCINT.P

Method : C:\HPCHEM\i\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing ; OFF Filtering; 5 Sampling ; 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks; 100 Stop Thrs : 0 Peak Location; TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation; 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % -max. total

1 6.326 136 140 147 rBV 54076 108113 1.43% 0.265% 2 6.427 147 151 160 rVV2 84353 213786 2.84% 0.524% 3 6.556 162 165 174 rW 43782 104114 1.38% 0.255% 4 6.675 174 178 191 rVB 58988 135029 1.79% . 0.331% 5 7.704 287 290 299 rBV 41553 102372 1.36% 0.251% 6 11.568 707 711 721 rBV 62286 145997 1.94% 0.358% 7 11.715 721 727 749 rBV 2112863 5230092 69.37% 12.814% 8 15.323 1113 1120 1136 rBV 3315076 7150970 94.85% 17.520% 9 20.602 1688 1695 1714 rBV 3427924 7539549 100.00% 18.472% 10 25.027 2170 2177 2189 rBV2 3218739 7023554 93.16% 17.208% 11 29.452 2654 2659 2666 rBV 212884 418845 5.56% 1.026% 12 29.571 2666 2672 2680 rVB 57395 112709 1.49% 0.276%' 13 30.645 2783 2789 2796 rBV 86057 170627 2.26% 0.418% 14 31.591 2887 2892 2897 rBV 168467 331615 4.40% 0.812% 15 31.682 2897 2902 2909 rVB 159908 332832 4.41% ,0.815% 16 32.674 3005 3010 3017 rBV 158898 328748 4.36%' 0.805% 17 —3 3 V0 6 0 —3-044—3 0 52 3070 -rBV2 -2287850-- 566837 0^7 5T18 %^ 13 T8 8'8 %' 18 33.629 3106 3114 3124 rBV 170152 389851 5.17% 0.955% 19 34.556 3210 3215 3224 rVB 124774 267367 3.55% 0.655% 20 35.446 3306 3312 3322 rBV 97137 229536 3.04% 0.562% 21 36.309 3400 3406 3416 rBV 49606 140505 1.86% 0.344% 22—37.163- 3490 3499 3513-rBV2-1585197- --4671010—61v95%--ll'.-444%

Sum2of2LQQrrected:rarea‘'s ;2iS24'081559r7Z

23799.D NP103001.M Thu Nov 01 13:16:28 2001

NYC-WTC_000089316

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NYC-WTC_000089316Source: NYC Law Department, mirrored locally

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