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GC/MS analysis results for sample AD23498, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23498 conducted on October 19, 2001.

NYC-WTC_000088774–000088798

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1601\23498.D Vial; 6 Acq On : 16 Oct 2001 7:07 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs ; 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.387 143 147 152 rBV 21040 40446 1.46% 0.230% 2 6.488 154 158 169 rW 34390 87551 3.16% 0.498% 3 6.626 169 173 182 rW 16173 39876 1.44% 0.227% 4 6.736 182 185 193 rVB 23490 50047 1.81% 0.285% 5 7.214 230 237 243 rBV2 9203 27787 1.00% 0.158% 6 11.620 712 717 727 rBV 23334 54606 1.97% 0.310% 7 11.758 727 732 752 rW 793019 2006589 72.41% 11.410% 8 15.375 1119 1126 1143 rBV 1216257 2724390 98.31% 15.491% 9 20.654 1694 1701 1714 rBV 1251777 2771308 100.00% 15.758% 10 25.088 2177 2184 2197 rBV2 1146117 2591937 93.53% 14.738%

11 29.504 2658 2665 2673 rBV 189425 377030 13.60% 2.144% 12 29.623 2673 2678 2686 rW 58016 112757 4.07% 0.641% 13 29.751 2688 2692 2699 rVB2 29028 57090 2.06% 0.325% 14 30.706 2790 2796 2803 rBV 83822 169511 6.12% 0.964% 15 31.643 2893 2898 2904 rBV 152293 310285 11.20% 1.764% 16 31.734 2904 2908 2918 rW 170631 346877 12.52% 1.972% -17—32.735- 3009-3017 -3030 rBV 160366 -346369’—1-2-50%- -Tt970%— 18 33.121 3052 3059 3075 rBV2 979057 2293876 82.77% 13.043% 19 33.690 3112 3121 3138 rBV 189603 408289 14.73% 2.322% 20 34.608 3215 3221 3232 rBV 130622 294999 10.64% 1.677% 21 35.498 3312 3318 3330 rBV 102037 244782 8.83% 1.392% 22 36.361 3407 3412 3424 rBV 52834 148668 5.36% 0.845% 23 37.233 3499 3507 3529 rBV2 693582 2049449 73.95% 11.653% 24 38.363 3623 3630 3635 rBV4 9214 32065 1.16% 0.182%

Sum of corrected areas: 17586584 23498 .D- NP09-1-10-1.M----- Thu-Oct 18 10:10:22- 2001

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