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GC/MS analysis results for sample AD23501, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23501 conducted on October 19, 2001.

NYC-WTC_000088853–000088879

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1601\23501.D Vial: 9 Acq On : 16 Oct 2001 10:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak. Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.148 9 12 25 rVB2 11172 34026 1.22% 0.190% 2 6.388 143 147 153 rBV 22961 46640 1.67% 0.260% 3 6.489 154 158 167 rW 38306 94694 3.38% 0.529% 4 6.626 169 173 181 rW 18398 43717 1.56% 0.244% 5 6.736 181 185 196 rVB 27193 60537 2.16% 0.338% 6 11.620 715 717 727 rVB 22793 45823 1.64% 0.256% 7 11.758 727 732 746 rBV 820833 1994215 71.24% 11.135% 8 15.375 1119 1126 1145 rBV 1191880 2749406 98.22% 15.351% 9 20.654 1694 1701 1713 rBV 1285685 2799217 100.00% 15.629% 10 25.079 2177 2183 2196 rBV2 1183031- 2595874 92.74% 14.494% 11 29.504 2660 2665 2673 rBV 211802 420892 15.04% 2.350% 12 29.623 2673 2678 2685 rVB 65872 129199 4.62% 0.721% 13 29.752 2685 2692 2699 rBV 27710 54895 1.96% 0.307% 14 30.697 2791 2795 2803 rBV2 97074 209237 7.47% 1.168% 15 31.643 2893 2898 2904 rBV 178710 350604 12.53% 1.958% 16 31.734 2904 2908 2919 rW 196890 399729 14.28% 2.232% 17—32-.-7-3-5—301-1-3017 3028 rBV----- 178645-------- 393777- -14.07%------2-7199% 18 33.121 3051 3059 3077 rBV2 971785 2240819 80.05% 12.512% 19 33.690 3114 3121 3134 rBV 210767 456591 16.31% 2.549% 20 34.608 3210 3221 3234 rBV 156377 350120 12.51% 1.955% 21 35.498 3313 3318 3330 rBV 121055 285673 10.21% 1.595% 22 36:.361 -3404 3412 3423 rBV 68036 190847 6.82% 1.066% -- 23 37.233 3498 3507 3512 rBV2 659317 1878854 67.12% 10.491% 24 38.363 3624 3630 3637 rBV2 13304 50389 1.80% 0.281% -25 3 9.-61-1- -375-7-3 766- 3772 rBV5 7813 —34156- -1-22% 0.191%

- Sum-of-corrected areas? 17909931 23501.D NP091101.M Thu Oct 18 10:21:14 2001

NYC-WTC_000088858

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NYC-WTC_000088858Source: NYC Law Department, mirrored locally

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