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GC/MS analysis results for sample AD23497, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.

NYC-WTC_000088753–000088773

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1601\23497.D Vial: 5 Acq On : 16 Oct 2001 6:08 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing -. OFF Filtering: 5. Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal ; TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.138 8 11 21 rVB2 11262 27104 1.05% 0.192% 2 6.378 142 146 151 rBV 21988 40905 1.58% 0.290% 3 6.479 154 157 168 rW 33827 91264 3.52% 0.647% 4 6.617 169 172 18 0 rW 17770 39274 1.51% 0.279% 5 6.727 180 184 194 rVB 24440 56112 2.16% 0.398% 6 10.215 557 564 572 rBV2 12225 29616 1.14%’ 0.210% 7 10 .426 583 587 595 rBV 11303 26222 1.01% 0.186% 8 11.629 713 718 727 rBV 21217 48721 1.88% 0.346% 9 11.767 727 733 751 rBV 756453 1886685 72.77% 13.380% 10 15.375 1120 1126 1139 rBV 1156169 2557386 98.64% 18.137% 11 20.653 1694 1701 1716 rBV 1194491 2592760 100.00% 18.387% 12 25.078 2177 2183 2193 rBV2 1065866 2387523 92.08% 16.932% 13 29.512 2661 2666 2673 rVB 23126 45906 1.77%: 0.326% 14 30.706 2791 2796 2803 rVB 16036 30467 1.18% 0.216% 15 31.642 2894 2898 2904 rBV 19153 35879 r.38% 0.254% 16 31.734 2904 2908 2916 rVB 32897 65853 2.54% 0.467% .17. _3 2.. -7.3.4- -3 011.3 01-7-3 02 3-rBV- -29526 -6-3004- 2.43%- - 0^.447% 18 33.120 3052 3059 3081 rBV2 946345 2102273 81.08% 14.909% 19 33.689 3112 3121 3128 rBV3 33469 76230 2.94% 0.541% 20 34.607 3217 3221 3227 rBV2 19788 42994 1.66% . 0.305% 21 35.498 3312 3318 3327 rBV2 14359 39962 1.54% 0.283% 22 37.233 3498 3507 3523 rBV2 636107 1814625 69.99%, 12.869%

—Sum-of—corrected areas: 14100765 23497.D NP091101.M Thu Oct 18 10:07:18 2001

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NYC-WTC_000088758Source: NYC Law Department, mirrored locally

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