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GC/MS analysis results for sample AD22914, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22914 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087540–000087561

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File C:\HPCHEM\1\DATA\OCT0 201\22914.D Vial: 4 Acq On 2 Oct 2001 5:03 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 . Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.381 142 146 154 rBV 26452 62153 1.77% 0.316% 2 6.482 154 157 167 rW 43275 117221 3.34% 0.596% 3 6.619 169 172 17 9 rW 20503 49012 1.40% 0.249% 4 6.739 181 185 193 rVB 28096 64832 1.85% 0.330% 5 11.641 715 719 729 rVB 26936 62939 1.79% 0.320% 6 729 735 752 rBV 952979 2460733 70.08% 12.516% 7 ^t5-.-3^96 1122 1128 1146 rBV 1565852 3369906 95.97% 17.140% 8 <2-©t-6B4- 1697 1704 1719 rBV 1663537 3511319 100.00% 17.859% 9 2180 2187 2199 rBV2 1437762 3264431 92.97% 16.603% 10 27.110 2398 2404 2414 rBV 75475 140204 3.99% 0.713% pLiHa 11 29.533/ 2662 2668 2674 rBV 108445 197492 5.62% 1.004% 12 29.653 2677 2681 2687 rVB 19352 37322 1.06% 0.190% 13 30.727 2793 2798 2804 rVB 28858 55485 1.58% 0.282% 14 31.672 / 2896 2901 2906 rBV 81616 154237 4.39% 0.784% 15 31.764/2906 2911 2916 rVB 58695 115863 3.30% 0.589%

16 ^.756-^ 3013 3019 3025 rBV 59569 122678 3.49% 0.624% 17 35>3r6^ 3055 3063 3082 rBV2 1183894 2868987 81.71% 14.592% 18 33.720^ 3116 3124 3130 rBV2 69156 151246 4.31% 0.769% 19 34.638/ 3219 3224 3231 rVB 53918 110377 3.14% 0.561% 20 35.528»/ 3316 3321 3329 rBV 45651 96854 2.76% 0.493% 21 36.391/ 3410 3415 3422 rBV 28214 65793 1.87% 0.335% 22 37^-373. 3502 3511 3528 rBV2 866798 2582392 73.54% 13.134%

Sum of corrected areas: 19661476 22914.D NP091101.M Wed Oct 03 09:48:46 2001

NYC-WTC_000087545

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