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GC/MS analysis results for sample AD23321, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23321 conducted on October 15, 2001.

NYC-WTC_000088237–000088262

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C;\HPCHEM\1\DATA\OCT1201\23321 .D Vial: 14 Acq On ; 12 Oct 2001 2:50 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Smoothing ; OFF Filtering: 5 Sampling : 1 Min Area; 1 % of largest Peak Start Thrs; 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP ’

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.384 142 146 153 rBV 21698 41057 1.31% 0.215% 2 6.494 153 158 168 rVV2 33075 87484 2.80% 0.459% 3 6.623 168 172 179 rW 19957 40002 1.28% 0.210% 4 6.733 180 184 192 rVB 27125 56600 1.81% 0.297% 5 11.626 713 717 726 rBV 25261 57691 1.84% 0.302% 6 11.764 726 732 752 rBV 931223 2204058 70.47% 11.553% 7 15.371 1118 1125 1142 rBV 1315597 3047290 97.44% 15.974% 8 20.659 1693 1701 1712 rBV 1363585 3127458 100.00% 16.394% 9 25.084 '2175 2183 2194 rBV 1336203 2866784 91.66% 15.027% 10 29.509 2660 2665 2672 rBV 206180 391340 12.51% 2.051% 11 29.628 2672 2678 2686 rW 49754 103150 3.30% 0.541% 12 29.748 2686 2691 2697 rW 29759 61470 1.97% 0.322% 13 30.703 2788 2795 2803 rBV 86849 167267 5.35% 0.877% 14 31.639 2892 2897 2903 rBV 144673 300053 9.59% 1.573% 15 31.740 2903 2908 2914 rW 155849 328130 10.49% 1.720%

16 32.731 3007 3016 3028 rBV 167960 344525 11.02% 1.806% 17 33.117 3051 3058-3073 rBV2 1054511 2510957 80.29% 13.162% 18 33.686 3112 3120 3128 rBV 183354 400710 12.81% 2.100% 19 34.613 3216 3221 3230 rVB 133438 290428 9.2 9% 1.522% 20 35.495 3312 3317 3326 rBV 107632 254341 8.13% 1.333%

21 36.358 3405 3411 3421 rBV 62519 166743 5.33% 0.874% 22 37.230 3498 3506 3512 rBV2 765933 2180748 69.73% 11.431% 23 38.359 3624 3629 3640 rBV2 14244 48775 1.56% 0.256%

Sum of corrected areas: 19077061 23321.D NP091101.M Mon Oct 15 09:56:58 2001

NYC-WTC_000088242

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NYC-WTC_000088242Source: NYC Law Department, mirrored locally

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