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GC/MS analysis results for sample AD23652, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23652 conducted on October 16, 2001.

NYC-WTC_000089045–000089058

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089057
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23652.D ■Vial: 4 Acq On : 15 Oct 2001 2:27 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 ; MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *********************************************************'************ Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area’ Relative to ISTD R.T. 11.63 0.50 ug/1 48560 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qua I" 1 1,4-Dich^robenzene-d4 150 C6C12D4 003855-82-1 53 ' 2 Benzenajifine, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 27 3. Benzer^-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 4 Benze/amine, 2-methyl-5-nitro- 152 C7H8N2O2 000099-55-8 12 ^bundance / Scan 718 (11.630 min): 23652.D (-) m/z 149.90 100.00% i$o

253 115 78 TT-p-r 52 T 11.20 11.40 11.60 11.80 12.00 ' ' I ' ' '3? •• '. 11' 45 I. , ' I • 87 111 m/z 151.90 57.79% nZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 “m/rnTTgO 33793%

30 35 40 50 60 JU: 70 80 90. 100 110 120 130 140 150 160 Abundance #10129: Benzenamine, 2-methyl-4-nitro- 77 106 ■152'

11.20 11.40 11.60 11.80 12.00 ' 253 InTz 78705 22.06% 51 94

' ' I ' ' '' I'''' I' ■p" 30 40 50 60 70 80 90 100 110 120 130 140 150 160 -Abundance . — #9592: Benzene-1.2.3,4-d4-. 5.6-dichloro-— ^::r-1$0— 11^20^11^40^1 'eO^tsodzbo^ m/z""52700 16.15%’ 115 5000 52 78

35 87 I Tife-> 30 I 40 50 ' I ' ‘ 60 ' I ' 70 ' I ' ' ' ' I ' ■ ' ' I ' 80 90 . IH'I,,,. 100 110 120 130 140 150 160 11.20 11,40 11.60 11,80 12.00 ' ' I ' '

23652.D NP091101.M Tue Oct 16 15:02:35 2001 Page 5

' NYC-WTC_000089057

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NYC-WTC_000089057Source: NYC Law Department, mirrored locally

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