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GC/MS analysis results for sample AD23345, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23345 conducted on October 16, 2001.

NYC-WTC_000088556–000088584

Folder label: “GC/MS Scan 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0901\23345.D Vial: 17 . Acq On : 10 Oct 2001 4:57 am Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 20 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.41 ug/1 40001 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hex^ol 102 C6H14O 000623-37-0 83 2 SilaiJe, trimethyl- 74 C3H10Si 000993-07-7 53 3 3-P/ntanol, 2-methyl- 102 C6H14O 000565-67-3 38 4 3-Xentanol 88 C5H12O 000584-02-1 36 Abundance Scan 172 6.622 min): 23345.D (-) m/z 57705 1 07700% 59 55

552 73

43 39 6.20 6.40 6.60 6.80 7.00 I I 49 84 T 44 ............. m/z 55700 78.52% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531:3-Hexanol

55

5000 73 . ......... . 6.20 6.40 6,60 6.80 7.00 43 mTz 73.00 45.71% 39 i"'7'>iii....... . +4 I......... I'''' I'''' I'''' I'''' I' ‘' I Tl/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #331: Silane, trimethyl- 5(9 I I I I I I ' I I I I I I IT

73 6.20 6.40 6.60 6.80 7.00 aSS "m/^ 43.00 22.37%

. s..T. n/z-> Abundance ' I" " I" 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63561: 3-Penfanol, 2-methyl- 5|9 +t I'''' I" " I'''' I

6.20 AJ 6.40 6.60 6.80 7.00 "m/z 4T .05 21.21%

5000 73

31 55 45 69 .. 85 TTp-n-rp- 102 '' I " '' I'' " I'''' I Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00

23345.D NP091101.M Thu Oct 11 13:09:38 2001 Page 3

NYC-WTC_000088565

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