GC/MS analysis results for sample AD23360, Oct 16 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT0901\23360.D Vial; 18 Acq On : 10 Oct 2001 5:55 am Operator; 209 GALOS Sample ; gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 6.61 0.55 ug/1 50861 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H14O 000623-37-0 83 2 Silane,/^ /£rimethyl- 74 C3H10Si 000993-07-7 59 3 3-Pe: X^nol 88 C5H12O 000584-02-1 59 4 3-Pi ■tanol, 2-methyl-____________ 102 C6H14O 000565-67-3 38 4bundanci Scan 171 (6.613 min): 23360.D (-) m/z 5^700 100.00% 50

73 5000 43

6.20 6.40 6.60 • 6.80 7.00 85 , I 53 4+ +t 100 rrp-rrrp-rrrj m/z 55.00 78.86% tt/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63531:3-Hexanol 50

5000- 73 6.20 6.40 6.60 6.80 7.00 43 m/^ 73.00 51.07%

..... 'I I'''' I'''' I Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ^bundance #331: Silane, trimethyl- 50

73 6.20 6.40 6.60 6.80 7.00 5000 m/^ 43.00 32.54%

45 I I'''' I'''' 1 ....... J,.......|illl| +t I''' ‘ 1'''' I''' ‘ I n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62943:3-Pentanol I ' ‘ ' I ' ' ' ' I ‘ ' I ' ' 50 6.20 6.40 6.60 6.80 7.00 m/^ 41.05 23.46% 31 5000 27 41

" ' I' ’ IH .II■."I■,I■I■11II nn/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

23360.D NP091101.M Thu Oct 11 13:13:03 2001 Page 3

NYC-WTC_000088594