GC/MS analysis results for sample AD23797, Nov 1 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3 001\23797.D Vial: 17 Acq On : 31‘Oct 2001 6:07 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

6.56 0.48 ug/1 71452 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolFoinn CAS# Qual

1 3-Hexanj 102 C6H14O 000623-37-0 90 2 3-Pen' /anol, 2-methyl- 102 C6H140 000565-67-3 45 3 3-Pe, hanol 88 C5H12O 000584-02-1 42 4 3- xanol, 5-methyl -_________________ 116 C7H16O 000623-55-2 38 4bundan<!!B Scan 165 (6.557 min): 23797.D (-) m/z 5.9.05 100.00% 5b

5000 73 43 I 1 I . . . . ( I r f 1 I , , , . I . . . I I . 620 6.40 6.60 6.80 7.00 4; ,.......... M................ 1W............. in/z 55.00 91.80% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531:3-Hexanol 5|9

5000 73 6.20 6.40 6.60 6.80 7.00 43 m/z 73.00 44.81%

TiZz-> +t +t +u + r+ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 flibundance#63561:3-Pentanol, 2-methyl- I'"' I" 111" 111"" I"" I

. I ■ 5b I , I , I , , I , , , 'T~?VA.|-T-r-,-,-|-r

6.20 6.40 6.60 6.80 7.00 5000 73 m/z 43.00 30.99% 31 . ,45 4 l"■.|'"l|. '85 102 I I H 11 !■ ■ ■ ■ I " I. I ■ " 11 ■ ■ " I 1 1 ■ 1 I TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance “ #62943:3-Pentanol _________ - sb -•n 6 20 --^6 40_ ^6 60 .6 80—7 0b m/z 41.’6 5 '20.23% 31 5000

41

TnTrrrrrWrtTTTTTTTTTtrU " I'''' I' il/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ' ' 6.40' 'e.eo' 6.80' '7.60

23797.D NP103001.M Thu Nov 01 12:04:03 2001 Page 3

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