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GC/MS analysis results for sample AD23343, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23343 conducted on October 16, 2001.

NYC-WTC_000088535–000088555

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088553
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23343.D Vial: 16 Acq On : 10 Oct 2001 3:59 am Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Benzene, l-nitro-2-(octyloxy)- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 35.66 1.64 ug/1 135080 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, lxiiitro-2-(octyloxy) - 251 C14H21NO3 037682-29-4 17 2 [1,1'-Biplienyl]-4-ol, 3-amino- 185 C12H11NO 001134-36-7 16 3 Butyl jdrtrate 360 C18H32O7 000077-94-1 16 4 1-Deqene, 2,4-dimethyl- 168 C12H24 055170-80-4 16 Abundance '' Scan 3336 (35.664 min): 23343.D (-) m/z 185.10 100.00% 185

57 5000 70 112 43 83 98 I W- 125 143 166 203 297 __3540_J5W_35B0_3a00^ m/z 57.00 51.29% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #34102: Benzene, 1-nitro-2-(octyloxy)- 517

71 5000 83 112 .35.40 35.60 35.80 36.00 139 m/z TOTTO 40.53% I I I ' ' ' 11 vLu . I ,,, .................... ^1......... 251 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ^bundance #19199; [1,1’-Biphenyl]-4-ol, 3-amino- 1 5

35.40 35,60 35,80 36.00 5000 m/z 71710 39.66% A 156 139

-n/z-> ^bundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300

129 #50331: Butyl citrate 1$5 JU 35.40 35.60 35.80 36.00 m/z 112.10 33.18% 5000

57 259

■n/z-> I ' I ' ' ' ' I ' 40 60 87 80 111 , I ) ' ' ‘ ‘ I 143^^^ ' I''' 'I'''' I 100 120 140 160 180 200 220 240 260 280 300 213 X ... ( 7..... 35.40 35.60 35.80 36.00

23343.D NP091101.M Thu Oct 11 13:05:50 2001 Page 12

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NYC-WTC_000088553Source: NYC Law Department, mirrored locally

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