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GC/MS analysis results for sample AD23343, Oct 16 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23343 conducted on October 16, 2001.

NYC-WTC_000088535–000088555

Folder label: “GC/MS Scan 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23343.D Vial: 16 Acq On : 10 Oct 2001 3:59 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Tetratriacontane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 34.61 0.53 ug/1 49254 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetratriacontane 479 C34H70 014167-59-0 83 2 Heneicosane 296 C21H44 000629-94-7 80 3 Docosane 310 C22H46 000629-97-0 80 4 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 _____ 055282-11-6 80 Abundance Scan 3221 (34.608 min): 23343.D (-) m/z 57700 100.00% 5|7 A 85 5000

221 I I ^19 1 256 34.20 34.40 34.60 34.80 35.00

n/z-> 1 " r ’'' I'" h "'' I" " I" " I" " I" " I" " I 40 60 80 100 120140 160180 200 220 240 260 280 300 320 340 360 380 400 m/z71.00 85.91% Abundance #58265: Tetratriacontane 7

asa 85 M aat-^Aaa ■ vy'T/ArA papa VW- 34.20 34.40 34.60 34.80 35.00 Tn/z 43705 83.68% jljLljTlt/s. I > I ■ 11 111 > 11 . < rp .. 11 311 I" " I 367 410 p ... I.... I .-r.. I.... I Ti/z-> 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #42201: Heneicosane 5)7

85 34.20 34.40 34.60 34.80 35.00 550 niTz 84.95 59.08%

I 113 4.4

n/z-> JJXmX YTTTTJTrnTTrrrpTTTTTT 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380400 268 296 I ’ ” * I"'' r''' I" " I

Abundance #44318: Docosane aA Ma A

57 34.20 34.40 34.60 34.80 35.00 m/z 41.00 32761% 85 Slilil

jJjlXdLS. I rH i |Ti 11 J. iTi 11 nT| I« > ■ j > । I" " I 266 310 ' I " " I " I . I I I’l . I I . I I I H I I I I I 1 I I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 34:20 34.40 34.60 34.80 35.00

23343.D NP091101.M Thu Oct 11 13:05:46 2001 Page 10

NYC-WTC_bb0088551

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NYC-WTC_000088551Source: NYC Law Department, mirrored locally

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