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GC/MS analysis results for sample AD22913, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22913 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087517–000087539

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document ninrary yearen Compound Reporb Data File : C;\HPCHEM\1\DATA\OCT0201\22913.D Vial: 3 Acq On : 2 Oct 2001 4:04 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library- : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Heneicosane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.39 0.62 ug/1 87046 Perylene-dl2 37.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91 3 Heptacosane 380 C27H56 000593-49-7 91 4 Nonadecane 268 C19H40 000629-92-5 90 Abundance Scan 3414 (36.386 min): 22913.D (-) m/z 57700 100.00% 57

85 5000

4' 36 00 36.20 36.40 36.60 36.80 169 208 253 281 T+rrpTT-^JTfTTpTTTrpTTTpTTT-pTTTp-rrrpTTTp^ m/z 71.00 65.41% ttZz-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #42201: Heneicosane ft 57

85 5000 36 00 36.20 36.40 36.60 36.80 m/z 43.05 63.14%

'' I'' I" " I" " I" " I"' • I" " r "' I" " I' •'' I"'' I ” " r' *' I" P ‘" I' “' r ’' ‘ I" " I'' Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #50999: Eicosane, 7-hexyl- 57

36.00 36,20 36.40 36.60 36.80 5000 85 m/z 85.05 49.46%

___ 281 ^0 _ 11 a 11 fl I q 111.1• I p 111 j... 111. H-| I •• " I '• »* f" " I " HI II . . I• . H I I . I .I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #52248: Heptacosane 57 36 00 36.20 36.40 36.60 36.80 mZz 55700 22.52% 5000 85

I , 169 196 224 281 324 380 " I " " I " I " '' I " ‘ ' I n " I " " I " " 1 " ' I " ' ' I “ " I' " ' I ’ " ' I " T T tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 36.00 36.20 36.40 36.60 36.80

22913.D NP091101.M Wed Oct 03 09:31:25 2001 Page 13

NYC-WTC_000087536

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NYC-WTC_000087536Source: NYC Law Department, mirrored locally

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