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GC/MS analysis results for sample AD22913, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22913 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087517–000087539

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document oeuxcii eompouna Reporc Data File : C:\HPCHEM\1\DATA\OCT0201\22913.D Vial: 3 Acq On : 2 Oct 2001 4:04 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 .625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Triacontane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 35.52 0.88 ug/1 123648 Perylene-dl2 37.28 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Triacontane 422 C30H62 000638-68-6 91 2 Heneicosane 296 C21H44 000629-94-7 90 3 Octadecane, 2-methyl- 268 C19H40 001560-88-9 90 4 Heptadecane 240 C17H36 000629-78-7 90 Abundance Scan 3320 (35.523 min): 22913.D (-) m7z 56795 100.00% 7

85 5000

T-r-p-r-r-r-f JI 35.20 35.40 35.60 35.80 . , J , J,, |l J . ... 253 J281, m/z 71705 77742% n/z-> 40 60 80 100120140160180 200220 240260280 300320340 360380 400420 Abundance #55461: Triacontane 43

71 5000 35.20 35.40 35.60 35.80 m/z 43.00 65.66% 239 267 379 422 "'J"' ' I"'' I “ " I" " I" " i"' ‘ I'‘ " I" " I" " I “ " I" " I''" I" " I'" TiZz-> 40 60 80 100120140160180 200220 240260280 300320340 360380 400420 'Msundance #42201: Heneicosane 57 71 35.20 35.40 35,60 35.80 85 5000 m/z 85.00 49.98%

HIS I I JjljxL. _____________ 268 296 '"1"' I, n 11T.,, I, IT.(.... I... 1111., I.... 1. 11.1..., I,,., I....I,,, I,,. ' I" " I" " I"' n/z-> 40 60 80 100120140160180 200220 240260280 300320340360380 400420 Abundance #71947: Octadecane, 2-methyl- I Pl I 57 35.20 35.40 35.60 35.80 m/z55.00 23.35% 5000 85

I il I 141 183 J,^,,,253 TTTlTTfTTflTrtTyTVTTfTTTIYTTTTy^^ ■Tl/Z-> 40 60 80 100120140160180200220240260280300320340360380 400 420 35.20 35.40 35.60 35.80

22913.D NP091101.M Wed Oct 03 09:31:22 2001 Page 12

NYC-WTC_000087535

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NYC-WTC_000087535Source: NYC Law Department, mirrored locally

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