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GC/MS calibration data for TCLP method, Oct 2001

Machine-extracted title · confidence 100%

Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.

NYC-WTC_000087496–000087516

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\LB.D Vial: 2 Acq On : 2 Oct 2001 3:06 pm Operator: 209 GALOS Sample : 9/20 Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L Peak Number 1 3-Hexanone Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.60 ug/1 76825 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 lentative ID MW MolForm CAS# Qual

1 3-Hexanpne 100 C6H12O 000589-38-8 91 2 3-Penb^one, 2-methyl- 100 C6H12O 000565-69-5 47 3 But zle, 2,2-dimethyl- 86 C6H14 000075-83-2 36 4 3p )-Furanone, dihydro-2-methyl- 100 C5H8O2 003188-00-9 35 ^bund^ce Scan 146 (6.378 min): LB.D (-) m/z 43700 100700% 43 57

71 502 1CX)

6.00 6.20 6.40 6.60 6.80 ......J,.. .........‘"'I' ....... . r I ..... I' m/z 56.90 83.53% n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1528:3-Hexanone 57

29 71 502 6.00 6.20 6.40 6.60 6.80 100 m/z 71700 54.94% i" " I" " i" " H ............... I I..,... ...........................■- r p n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 /Xbundance #63398: 3-Pentanone, 2-methyl- 5(7 43 JkJ 6.00 6.20 6.40 6.60 6.80 5000 m/z 100.05 30.23% 100 71 A 85 I" ‘' I" " I" " I" " I ............... .11 p-rri 111111111 ■ I ■ 11111 M I ...... nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #732: Butane, 2,2-dimethyl- 43 57 6.00 6.20 6.40 6.60 6.80 71 m/z 41.00 23751% 29 5000

15 ............. I........ I ‘ 'I " "I" " I" " I" "I" "I" "I" " I' Tife-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

LB.D NP091101.M Wed Oct 03 10:09:44 2001 Page 1

NYC-WTC_000087502

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NYC-WTC_000087502Source: NYC Law Department, mirrored locally

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