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GCMS analysis results for sample AD24483, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.

NYC-WTC_000068763–000068777

Folder label: “GCMS Scan X 10/15/01 A 11/3/01

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Scanned page image, NYC-WTC_000068771
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0201\24483.D Vial: 22 Acq On : 3 Nov 2001 11:26 am Operator: 209 GALOS Sample : gc/ms unknown Inst J GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.31 0.54 ug/1 81358 1,4-Dichlorobenzene-d4 11.71 Hit# of Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H12O 000589-38-8 78 2 3-Pentanone, 2-methyl- 100 C6H12O 000565-69-5 42 3 3(2H)-Furanone, dihydro-2-methyl- 100 C5H8O2 003188-00-9 35 4 Butape, 2,2-dimethyl- 86 C6H14 000075-83-2 33 Abundance Scan 138 (6.313 min): 24483.D (-) m/z 43.00 100.00% 4)3 57

71 5000 100

6.00 6.20 KJ 6.40 6.60 . .... ?/:i|li Tnv.|l.i.|l 51 ...... ......... ...... m/z 57.00 96.29% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ^bundance #63357:3-Hexanone 46 57 29

5000 71 6.00 6.20 6.40 6.60 100 m/z 70.95 57.76% 85 t+ P nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63398: 3-Pentanone, 2-methyl- 5)7 43 6.00 6.20 6.40 6.60 5000 m/z 100.05 ^7771% 100

L L- 71 85 I"'' I'''' I''" I " ' r "' I " " I" " I ‘' I'' Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 '\bundance #63310: 3(2H)-Furanone, dihydro-2-methyl- 4)3 6.00 6.20 6.40 6,60 "mTz 41.00 26.90% 5000 72 100

49 57 I''" I'''' I p 'nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60

24483.D NP103001.M Fri Nov 09 15:03:06 2001 Page 1

NYC-WTC_000068771

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NYC-WTC_000068771Source: NYC Law Department, mirrored locally

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