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GC/MS calibration table for TCLP method, Oct 2001

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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.

NYC-WTC_000087132–000087155

Folder label: “508 Scan 9/18/01 9/27/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report ’ Data File C:\HPCHEM\1\DATA\OCT0101\LBE .D Vial: 5 Acq On 1 Oct 2001 5:38 pm Operator; 209 GALOS Sample 9/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling ; 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks; 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal ; TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max'. total 1 6.384 142 146 153 rBV 72066 150086 3.79% 0.651% 2 6.485 153 157 168 rW 97408 268153 6.77% 1.162% 3 6.623 168 172 18 0 rW 55396 130968 3.31% 0.568% 4 6.742 180 185 196 rVB 42708 101670 2.57% 0.441% 5 7.770 293 297 305 rBV 45343 112694 2.84% 0.488% 6 10.837 627 631 645 rBV 20550 60964 1.54% 0.264% 7 11.644 715 719 728 rVB 31985 75603 1.91% 0.328% 8 11.782 729 734 746 rBV 1113918 2795347 70.55% 12.116% 9 15.399 1121 1128 1145 rBV 1747154 3846462 97.08% 16.672% 10 20.687 1697 1704 1720 rBV 1838190 3962056 100.00% 17.173% 11 25.121 2180 2187 2198 rBV2 1646831 3705336 93.52% 16.060% 12 29.537 2663 2668 2674 rBV 175375 329818 8.32% 1.430% 13 29.656 2676 2681 2687 rW 36695 71795 1.81% 0.311% 14 29.785 2690 2695 2701 rVB 23024 44333 1.12% 0.192% 15 30.730 2793 2798 2805 rVB 53839 107794 2.72% 0.467% 16 31.676 2895 2901 2906 rBV 125674 252715 6.38% 1.095% 17 31.768 2906 2911 2918 rW 110746 217032 5.48% 0.941% 18 32.759 3014 3019 3025 rBV 104595 208771 5.27% 0.905% 19 33.163 3055 3063 3075 rBV2 1348508 3236979 81.70% 14.030% 20 33.714 3114 3123 3130 rBV 104724 233381 5.89% 1.012% 21 34.641 3219 3224 3232 rVB 69802 145324 3.67% 0.630% 22 35.532 3316 3321 3328 rVB 50411 106189 2.68% 0.460% 23 36.395 3410 3415 3421 rBV2 25677 56941 1.44% 0.247% 24 37.285 3503 3512 3530 rBV2 976064 2851247 71.96% 12.358%

Sum of corrected areas*. 23071658

LBE.D NP091101.M Wed Oct 03 14:40:51 2001

NYC-WTC_000087136

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