Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
NYC-WTC_000087496–000087516Folder label: “GC/MS Scan 9/20/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT0201\LB.D Vial: 2 Acq On : 2 Oct 2001 3:06 pm Operator: 209 GALOS Sample : 9/20 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling ; 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location; TOP
If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5
Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 5.138 9 11 23 rVB 17970 46970 1.27% 0.222% 2 6.378 142 146 153 rBV 34333 76825 2.08% 0.363% 3 6.488 153 158 161 rBV 54801 107024 2.90% 0.506% 4 6.616 169 172 181 rVB 24613 53199 1.44% 0.252% 5 6.736 181 185 198 rVB 38000 88381 2.39% 0.418% 6 11.638 715 719 729 rVB 28778 69043 1.87% 0.326% 7 11.785 729 735 750 rBV 1042087 2566396 69.49% 12.136% 8 15.402 1122 1129 1146 rBV 1565980 3567297 96.59% 16.869% 9 20.690 1698 1705 1718 rBV 1635893 3693277 100.00% 17.465% 10 25.115 2180 2187 2199 rBV2 1586051 3443890 93.25% 16.286% 11 29.539 2663 2669 2675 rBV 133513 260921 7.06% 1.234% 12 29.650 2675 2681 2686 rBV 28538 54299 1.47% 0.257% 13 30.733 2793 2799 2805 rVB 44804 84270 2.28% 0.399% 14 31.669 2893 2901 2907 rBV 100989 204617 5.54% 0.968% 15 31.770 2907 2912 2922 rVB 85552 179169 4.85% 0.847% 16 32.762 3014 3020 3025 rBV 92217 183463 4.97% 0.868% 17 33.157 3056 3063 3078 rBV2 1308298 3048404 82.54% 14.415% 18 33.717 3117 3124 3131 rBV 110571 221588 6.00% 1.048% 19 34.635 3217 3224 3231 rBV 76980 168992 4.58% 0.799% 20 35.525 3316 3321 3329 rBV 68508 147163 3.98% 0.696% 21 36.388 3411 3415 3421 rBV2 40955 93256 2.53% 0.441% 22 37.278 3503 3512 3531 rBV2 944832 2788267 75.50% 13.185%
Sum of corrected areas: 21146711
LB.D NP091101.M Wed Oct 03 10:09:37 2001
NYC-WTC_00008750b
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