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GC/MS analysis results for sample AD22549, September 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087022–000087043

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087041
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NYC 9/11 Public Portal Document

ary Search Compound Report Data File : C:\HPC .1\1\DATA\SEP26O1\22549 .D Vial: 3 Acq On : 26 Seo 101 12:17 pm Operator: GALOS Sample : GC/MS • Tnown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Par ••5: LSCINT.P Quant Method : C;\h CHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 203 ’5/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\r ?ABASE\NBS75K.L ****************** '********************************************** Peak Number 12 He uacontane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.78 0.72 ng/u 54634 Chrysene-dl2 33.30

Hit# of 5 Tent- -e ID MW MolForm CAS# Qual

nJ Hexatriacentane 507 C36H74 000630-06-8 8 Tricosane 324 C23H48 000638-67-5 .83 3 Tetracosane 338 C24H50 000646-31-1 83 4 Pentatriacontan 493 C35H72 000630-07-9 83 Abundance 65 (34.777 min): 22549.D (-) m/z SYTTO 100.00% 7 A

num 85

34 40 34.60 34.80 35.00 35.20 I m/z 43.10 68.08% I 2^ ' 300 350 ' 4TO ' ' 450 ' 500 Ti/z->______ 50 ' 150 Abundance 3136: Hexatriacontane 57

iBiiil I ' ' ' ' I 85 34 40 34.60 34.80 35.00 35.20 m/z 71705 61.14% 239 379 407 <^5 478 506 tVz-> 50 100 150 250 300 350 400 450 500 Abundance #73318: Tricosane 43

71 34 40 34.60 34.80 35.00 35.20 5000 m/z 85.05 40.42%

I , 127 ! . .... ......................... n/z->______ 50 100 150 250 300 350 400 450 500 Abundance .‘^73543: Tetracosane 7 34.40 34.60 34.80 35.00 35.20 m/z 41710 2^767%

Blilil 85

.... 294 338................. ■n/z-> 50 100 150 250 300 350 400 450 500 34.40 34.60 34.80 35.00 35.20

22549.D NP072501.M Mon Oct 01 14:40:33 2001 Page 12

NYC-WTC_000087041

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NYC-WTC_000087041Source: NYC Law Department, mirrored locally

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