GC/MS analysis results for sample AD22549, September 2001

NYC 9/11 Public Portal Document

Li ary Search Compound Report Data File : C:\nr 1\1\DATA\SEP26O1\22549.D Vial: 3 Acq On • 26 S '.- 501 12:17 pm Operator: GALOS Sample : GC/KS mown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integrat7.ion Pi 3: LSCINT.P

Quant Method ; C: CHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 20; 35/TCLP calibration table 7/25/01 Cl IS 5 Library- : C:' rABASE\NBS75K.L *******************-;. * ********************************************** Peak Number 13 Tri' itane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 35.66 0.59 ng,c 33892 Perylene-dl2 37.41

Hit# of 5 Ten'- ^e ID MW MolForm CAS# Qual

1 Triacontane 422 C30H62 000638-68-6 83'< 2 Heptacosane 380 C27H56 000593-49-7 83 / 3 Tricosane 324 C23H48 000638-67-5 83 / 4 Dodecane, 2-metIr. 6-propyl-________ 226 C16H34 055045-08-4 83 / Abundance '1 (35.657 min): 22549.D (-) m/z57710 100.00% 57

5000 85

35.40 35.60 35.80 36.00 H I JI I..... ..... 207 m/z 43.10 76760% r"'I""I tnfe-> 40 60 SO 100120140 . 9 200 220 240 260 280 300 320 340 360 380 400 420 Abundance 755461: Triacontane 43

71 5000 35.40 35.60 35.80 36.00 I m/z 71.05 60714%

Ti/2-> ' ‘ I " ' 1 I'"' I-

40 60 8t.' i 0012014-: ;■ 127 239 267 I .. I ■ I . . H] I I I . I 1. ) 200 220 240 260 280 300 320340 360 380400 420 yrrrrrrrrrj- 379 422

Abundance ■74082: Heptacosane 43

71 35.40 35.60 35.80 36.00 5000 m/z 85.15 39.41%

.<9 127 1'3 211 253 353 380 TT^TrA^rr ■'■m 'O' Uf|„tTTtTTTTT.r.-r '"' I'"' I'' nyz-> 40 60 80 100120140'- " 0 200 220 240 260 280 300 320 340 360 380 400 420 Abundance //73318; Tricosane 3 35.40 35.60 35.80 36.00 m/z 55.10 25751% 71 A 5000

Ll.Lu . .'7 1P3 211 >> I I I I I I I I ■' T I |‘ I I I ‘Il I 296 324 I'' "I'''' 11'" I" " I"' 11 35I4O 35'60 35.'80 36.'00 Tl/2-> 40 60 80 100120140 160180 200 220 240260 280 300 320340 360380400420

22549.D NP072501.) Mon Oct 01 14:40:34 2001 Page 13

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