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GC/MS analysis results for sample AD22549, September 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087022–000087043

Folder label: “508 Scan 9/18/01 9/27/01

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Scanned page image, NYC-WTC_000087040
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

T '.ary Search Compound Report

Data File : C:\KP< -1M\1\DATA\SEP26O1\22549.D Vial: 3 Acq On : 26 S 101 12:17 pm Operator: GALOS Sample : GC/M -.nown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration P; 3: LSCINT.P Quant Method : C: ■CHEM\1\METHODS\NP072501 .M (RTE Integrator) Title : 208 /25/TCLP calibration table 7/25/01 Cl IS 5 Library : C:\I TABASE\NBS75K.L ********************* *********************************************** Peak Number 11 Eicc.' ■le Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.86 1.38 ng.' 105173 Chrysene-dl2 33.30

Hit# of 5 Tei..t .^e ID MW MolForm CAS# Qual

k^Eicosane 282 C20H42 000112-95-8 90 (^Tetracosane 338 C24H50 000646-31-1 90 3'Nonadecane 268 C19H40 000629-92-5 90 4 Pentacosane ______________________ 352 C25H52 000629-99-2 83 Abundance St. ■ 65 (33.860 min): 22549.D (-) m/z SYTTO 100.00% 57

43 71

5000 85

33.60 33.80 34.00 34.20 207 I'''' I p-Vn-p-m-f m/z 43710 68793% 40 60 80 100 120 160 180 200 220 240 260 280 300 320 340 Abundance #72323: Eicosane 43 = 7

71 5000 85 33.60 33.80 34.00 34.20 m/z 71.05 63.48% ,, ^11312714 282 r ■‘"T p-n-rp-m-f ' I'''' I'''' 11''' I Tl/z-> 40 60 80 100 160 180 200 220 240 260 280 300 320 340 Abundance 173543: Tetracosane 43 5[7 71 T 33.60 33.80 34.00 34.20 5000- 85 m/z 85.05 33.55%

99 l| ('[^127 :55169183197

TiZz-> 40 J60 80 100 120 1 ■ ' 160 180 200 220 240 260 280 300 320 340 I'''' I'''' I'''' I' I ' ‘ ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I 294 I'''' I'''' I 338 I ’''' I ’

Abundance .771948: Nonadecane 4S 57 _3a60_3a80_340g_3420_^ m/z 55710 27.68% 71 lilial 85

,1 II , 156 196210225 268 ' ' I ' ' ' ' I ■ ' ' 'I ' ‘ . I . . . ; '' I'''' I ‘' r TiZz-> 40 60 80 100 120 1 160 180 200 220 240 260 280 300 320 340 33.60 33.80 34.00 34.20

22549.D NP072501.M Mon Oct 01 14:40:33 2001 Page 11

NYC-WTC_000087040

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NYC-WTC_000087040Source: NYC Law Department, mirrored locally

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