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GC/MS analysis results for sample AD22549, September 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD22549 conducted on September 27, 2001, identifying unknown compounds.

NYC-WTC_000087022–000087043

Folder label: “508 Scan 9/18/01 9/27/01

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NYC 9/11 Public Portal Document

Li .ary Search Compound Report Data File : C:\HP<: :EM\1\DATA\SEP26O1\22549.D Vial: 3 Acq On ; 26 Sep 2001 12:17 pm Operator: GALOS Sample : GC/MS T iknown Inst : GC/MS Ins Mise Multiplr; 1.00 MS Integration Par-^ i.s: LSCINT.P

Quant Method : C:V ?CHEM\1\METHODS\NP072501.M (RTE Integrator) Title : 2(n-- ;25/TCLP calibration table 7/25/01 Cl IS 5 Library : C: .TABASE\NBS75K.L

Peak Number 10 Hept .ecane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

32.91 1.14 ng/ 87255 Chrysene-dl2 33.30

Hit# of 5 Tent - - ' ve ID MW MolForm CAS# Qual

\L^eptadecane 240 C17H36 000629-78-7 83 2^Hexadecane 226 C16H34 000544-76-3 72 3 Decane, 2,2,8-t' :hyl- 184 C13H28 062238-01-1 42 4 Ether, hexyl pe; 172 C11H24O 032357-83-8 40 ^bundance 061 (32.906 min): 22549. D (-) m/z 57710 100.00% 57

43 71

J 5000 o5 I T 32.60 32.80 33.00 33.20 11 T-r-r-r-r-pr-T il m/z 43710 62.63% ■n/z-> 20 40 60 80 ) 120 140 160 180 200 220 240 A Abundance ■71191: Heptadecane 57 43

71 5000 85 32.60 32.80 33.00 33.20 I m/z 71.05 53.68% 4-r-j • 113 127 141 240 ft Ti/z-> 20 40 I60 . 80 0 120 140 160 180 200 220 240 Abundance #70789: Hexadecane 57 43 32.60 32.80 33.00 33.20 71 m/z 85.05 35.64% 5000

113 127................... ■n/z-> 20 40 60 80 '.'0 120 140 160 180 200 220 240 Abundance # .512: Decane, 2,2,8-trimethyl- 5'7 32.60 32.80 33.00 33.20 m/z 41‘.10 26.30%

5000

n/z-> 1 27^ 42 20 40 7L" 60 85 ' ’,7,..... 1S9 120 140 160 180 200 220 240 32.60 32.80 33.00 33.20

22549.D NP072501.M Mon Oct 01 14:40:32 2001 Page 10

NYC-WTC_000087039

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NYC-WTC_000087039Source: NYC Law Department, mirrored locally

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