VOC analysis results, sample AE12279, May 2002

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Data File : C:\HPCHEM\l\DATA\02MAY23\12284S, D Vial 1 Acq On : 23 May 2002 4:14 pm Operator 201-wb Sample : spk 2 0 Inst GC/MS Ins Mise Multiplr 1.00 MS Integration Params: GAS6.P Quant Time: May 31 11:55 2002 Quant Results File: HP051702.RES Quant Method : C:\HPCHEM\1\METHODS\HP051702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri May 31 11:43:42 2002 Response via : Initial Calibration DataAcq Meth : HP051702

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-DIFLUOROBENZENE 15.07 114 1471493 5.00 ug/L 0.03 24) CHLOROBENZENE-D5 21.72 117 1420348 5.00 ug/L 0.02 52) 1,4-DICHLOROBENZENE-D4 26.92 152 711747 5.00 ug/L 0.03 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.30 65 643297 4.48 ug/L 0.03 Spiked Amount 5.000 Recovery = 89.60% 3) 4-BROMOFLUOROBENZENE 24.31 174 589449 5.68 ug/L 0.02 Spiked Amount 5.000 Recovery = 113.60% 25) TOLUENE-D8 18.42 98 1852649 4.78 ug/L 0.02 Spiked Amount 5.000 Recove27y 95.60% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.84 85 2004141 30.62 ug/L 98 6) VINYL CHLORIDE 5.56 62 1097696 29.68 ug/L 99 7) BROMOMETHANE 6.55 94 1105599 30.48 ug/L 100 8) CHLOROETHANE 6.70 64 1568014 35.65 ug/L 99 9) TRICHLOROFLUOROMETHANE 7.25 101 2452893 29.79 ug/L 99 12) ACETONE 8.21 43 685916 52.64 ug/L 98 13) 1,1-DICHLOROETHENE 8.56 61 2055373 19.43 ug/L 99 14) METHYLENE CHLORIDE 9.57 49 2127038 22.05 ug/L 94 15) METHYL TERT BUTYL ETHER 9.88 73 1518396 20.32 ug/L 97 16) TRANS-1,2-DICHLOROETHENE 10.23 61 2473977 23.07 ug/L 89 17) 1,1-DICHLOROETHANE 11.14 63 2723206 23.45 ug/L 97 18) 2-BUTANONE (MEK) 11.95 43 918434 93.84 ug/L 94 19) 2,2-DICHLOROPROPANE 12.34 77 2100994 22.30 ug/L 99 20) CIS-1,2-DICHLOROETHENE 12.45 96 1415230 22.46 ug/L 98 21) CHLOROFORM 12.77 83 2658487 21.39 ug/L 99 2 2) BROMOCHLOROMETHANE 13.16 49 1156943 23.67 ug/L 96 23) 1,2-DICHLOROETHANE 14.51 62 1918160 20.65 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.67 97 2070132 17.93 ug/L 99 27) 1,1-DICHLOROPROPENE 14.00 75 2200338 20.46 ug/L 100 28) CARBON TETRACHLORIDE 14.25 117 1755244 18.47 ug/L 99 29) BENZENE 14.59 78 5069312 21.83 ug/L 100 30) TRICHLOROETHENE 15.87 95 1534526 19.83 ug/L 98 31) 1,2-DICHLOROPROPANE 16.23 63 1349265 21.53 ug/L 98 32) DIBROMOMETHANE 16.91 174 599927 19.75 ug/L 94 33) BROMODICHLOROMETHANE 16.75 83 1863230- 20.44 ug/L 100 34) 2-CHLOROETHYL VINYL ETHER 17.23 63 55818 4.62 ug/L 97 35) METHYL ISO-BUTYL KETONE 17.30 58 754296 96.08 ug/L 99 36) CIS-1,3-DICHLOROPROPENE 17.84 75 1885848 21.37 ug/L 99 37) TOLUENE 18.59 91 5298995 22.36 ug/L 100 38) TRANS-1,3-DICHLOROPROPENE 18.88 75 1439955 20.12 ug/L 100 39) 1,1,2-TRICHLOROETHANE 19.26 97 732391 20.06 ug/L 99 40) TETRACHLOROETHENE 20.04 166 1518080 21.73 ug/L 98 41) 1,3-DICHLOROPROPANE 19.80 76 1486398 20.97 ug/L 98 42) DIBROMOCHLOROMETHANE 20.48 129 984065 22.28 ug/L 94 43) 1,2-DIBROMOETHANE 20.94 107 758758 19.96 ug/L 99 44) CHLOROBENZENE 21.81 112 3246092 22.61 ug/L 99 45) 1,1,1,2-TETRACHLOROETHANE 21.86 131 1104969 19.93 ug/L 95 46) 2-HEXANONE 19.15 43 1427306 94.99 ug/L 99 47) ETHYLBENZENE 21.86 91 6323203 22.65 ug/L 99 48) P & M-XYLENE 22.01 106 4074627 45.48 ug/L 97 49) 0-XYLENE 22.98 91 5047820 23.20 ug/L 97 {#) = qualifier out of range (m) = manual integration 12284S.D HP051702.M Fri May 31 11:56:24 2002 Page 1

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