VOC analysis results, sample AE12738, June 4 2002

NYC 9/11 Public Portal Document

Data File C:\HPCHEM\l\DATA\02june04\0604R5 .D Vial: 4 Acq On 4 Jun 2002 2:31 pm Operator: 201-wb Sample ref 5 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: GAS6.P Quant Time: Jun 4 15:10 2002 Quant Results File: HP052902.RES Quant Method : C:\HPCHEM\1\METHODS\HP052902.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Fri May 31 14:34:13 2002 Response via : Initial Calibration DataAcq Meth : HP052902

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.09 114 1660795 5.00 ug/L -0.02 24) CHLOROBENZENE-D5 21.75 117 1551366 5.00 ug/L 0.00 52) 1,4-DICHLOROBENZENE-D4 26.93 152 802358 5.00 ug/L 0.00 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 698311 4.65 ug/L -0.02 Spiked Amount 5.000 Recovery = 93.00% 3) 4-BROMOFLUOROBENZENE 24.34 174 610999 4.62 ug/L 0.00 Spiked Amount 5.000 Recovery = 92.40% 25) TOLUENE-D8 18.45 98 2040688 5.22 ug/L -0.02 Spiked Amount 5.000 Recovery = 104.40% Target Compounds Qvalue ■ 4) DICHLORODIFLUOROMETHANE 4.85 85 266012 4.49 ug/L 97 5) CHLOROMETHANE 5.37 50 371031 4.03 ug/L 100 6) VINYL CHLORIDE 5.60 62 289816 6.08 ug/L 95 7) BROMOMETHANE 6.58 94 141121 5.43 ug/L 98 8) CHLOROETHANE 6.71 64 217752 5.10 ug/L 97 9) TRICHLOROFLUOROMETHANE 7.26 101 391417 5.54 ug/L 99 10) Isopropyl Alcohol 7.87 45 32652614 21216.47 ug/L 97 12) ACETONE 8.24 43 284030 16.39 ug/L 97 13) 1,1-DICHLOROETHENE 8.60 61 338266 2.83 ug/L 99 14) METHYLENE CHLORIDE 9.61 49 •366456 3.30 ug/L 93 15) METHYL TERT BUTYL ETHER 9.91 73 272868 3.18 ug/L 99 16) TRANS-1,2-DICHLOROETHENE 10.27 61 366768 2.99 ug/L 95 17) 1,1-DICHLOROETHANE 11.16 63 458728 3.34 ug/L 98 18) 2-BUTANONE (MEK) 11.99 43 152191 11.73 ug/L 100 19) 2,2-DICHLOROPROPANE 12.38 77 349277 3.40 ug/L 98 20) CIS-1,2-DICHLOROETHENE 12.47 96 278676 3.87 ug/L 90 21) CHLOROFORM 12.81 83 549028 3.89 ug/L 99 2 2) BROMOCHLOROMETHANE 13.18 49 210921 3.48 ug/L 88 23) 1,2-DICHLOROETHANE 14.53 62 379215 3.85 ug/L 96 26) 1,1,1-TRICHLOROETHANE 13.69 97 390252 3.89 ug/L 100 27) 1,1-DICHLOROPROPENE 14.02 75 350859 3.70 ug/L 97 28) CARBON TETRACHLORIDE 14.29 117 327561 3.91 ug/L 98 29) BENZENE 14.63 78 951942 4.10 ug/L 98 3 0) TRICHLOROETHENE 15.89 95 296038 4.26 ug/L 99 31) 1,2-DICHLOROPROPANE 16.25 63 253863 4.16 ug/L 98 32) DIBROMOMETHANE 16.93 174 125553 4.47 ug/L 87 3 3) BROMODICHLOROMETHANE 16.78 83 386213 4.42 ug/L 100 34) 2-CHLOROETHYL VINYL ETHER 17.26 63 58872 3.26 ug/L 90 35) METHYL ISO-BUTYL KETONE 17.34 58 139608 16.16 ug/L 98 36) CIS-1,3-DICHLOROPROPENE 17.87. 75 332112 4.14 ug/L 99 37) TOLUENE 18.62 91 1133109 4.68 ug/L 96 38) TRANS-1,3-DICHLOROPROPENE 18.91 75 254685 4.44 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.28 97 173144 4.86 ug/L 98 40) TETRACHLOROETHENE 20.07 166 315292 4.71 ug/L 97 41) 1,3-DICHLOROPROPANE 19.81 76 .312859 4.48 ug/L 99 42) DIBROMOCHLOROMETHANE 20.51 129 204826 4.72 ug/L 93 43) 1,2-DIBROMOETHANE 20.97 107 153955 4.35 ug/L 92 4 4) CHLOROBENZ ENE 21.84 112 772486 5.04 ug/L 97 45) 1,1,1,2-TETRACHLOROETHANE 21.89 131 258646 5.06 ug/L 97 46) 2-HEXANONE 19.18 43 262733 15.60 ug/L 96 47) ETHYLBENZENE 21.87 91 1447619 5.01 ug/L 98 (#) = qualifier out of range (m) = manual integration 0604R5.D HP052902.M Tue Jun 04 15:10:17 2002 Page 1

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